Chinese Journal of Lasers, Volume. 49, Issue 19, 1902002(2022)

Application of Synchrotron Radiation and Neutron Diffraction Technologies in Additive Manufacturing

Hongwen Deng1,2,4, yi Zhang2,3,4, Aodong Quan1,2,4, Yudai Wang2,3,4, Haibo Tang2,3,4, and Xu Cheng2,3,4、*
Author Affiliations
  • 1School of Materials Science and Engineering, Beihang University, Beijing 100191, China
  • 2National Engineering Laboratory of Additive Manufacturing for Large Metallic Components and Engineering Research Center, Beihang University, Beijing 100191, China
  • 3Research Institute for Frontier Science, Beihang University, Beijing 100191, China
  • 4Beijing Engineering Technological Research Center on Laser Direct Manufacturing for Large Critical Metallic Component, Beijing 100191, China
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    Figures & Tables(9)
    Time-series radiographs acquired during laser additive manufacturing (LAM) of Invar 36 single layer melt track. The effect of recoil pressure on metal powder movement and trajectory of pores under Marangoni convection were discovered[25]
    Controlling instability during metal additive manufacturing[47]. (a) X-ray images showing liquid breakup during laser melting of Al6061, where the broken liquid is indicated by dashed circle; (b) X-ray images showing laser melting of Al6061+4.4% TiC, the pressure in liquid is stable and the liquid will not break; (c) vapor depression depth and width evolution with time during laser melting
    Time-lapse images of samples at different numbers of cycles[113], where the first, second, and third rows show three-dimensional images of voids, virtual slice at neckdown position, and longitudinal section. (a) AlSi10Mg sample (HT105) tested at 250 ℃ and peak load of 105 MPa; (b) AlSi10Mg sample (RT260) tested at room temperature and peak load of 260 MPa
    Von Mises residual stress (RS) at the top of sample in thin-baseplate (TB) condition[117]
    Measurement of residual stress in metal components prepared by additive manufacturing. (a) Distribution of measurement points on the sample for neutron diffraction residual stress measurement[89]; (b) schematic of KOWARI neutron diffraction device for residual stress measurement in experiment[89]; (c) schematic of in-situ neutron diffraction experiment for measuring lattice strain[92]
    Evolution and analysis of solid-state phase transformation of additive manufacturing metal components. (a) Evolution of measured and calculated volume fraction of γ′ phase during thermal cycling[125]; (b) relationship between martensite phase volume fraction of tensile sample and true strain[82]
    Evolution of total dislocation density at three representative axial positions versus true strain[129] (RD: parallel to sonotrode rolling direction; TD: parallel to sonotrode vibration direction)
    • Table 1. Application of characterization methods based on synchrotron radiation (SR) in additive manufacturing

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      Table 1. Application of characterization methods based on synchrotron radiation (SR) in additive manufacturing

      TechniqueFacilityBeamlineMaterialMethodStudy field
      LPBFEuropean Synchrotron Radiation Facility(ESRF)

      ID19

      ID-31

      Ti6Al4V[20-22]

      Inconel 625[23]

      Imaging SR-XRD

      μ-CT

      Melt pool dynamics[21]

      Powder dynamics[20-21]

      Pore evolution[20]

      Phase transformation[22]

      Surface defects[23]

      LPBF

      Diamond

      Light Source

      I12-JEEPInvar 316L[24-26]Imaging

      Melt pool dynamics[24-26]

      Powder dynamics[24-26]

      Pore evolution[24-26]

      DEDDiamond Light SourceI12-JEEP

      SS316[27]

      Ti6Al2Sn4Zr2Mo[27]

      Inconel 718[28]

      Imaging SR-XRD

      Melt pool dynamics[27-29]

      Pore evolution[27]

      Phase transformation[28]

      Stress evolution[28]

      Micro-cracks evolution[28]

      LPBFAdvanced Photon Source(APS)

      32-ID-B

      35-ID

      2-BM

      Ti6Al4V[630-45]

      Al6061[313746-49]

      Al10SiMg[303440-4248-51]

      174 PH SS[52]

      316L[5053]

      AISI 4140

      Inconel 718[3054]

      SS316[4654]

      Al alloys[55]

      Ti10V2Fe3Al[56]

      Imaging

      SR-XRD

      Dynamic X-ray radiography

      Melt pool dynamics[63032-3335-4143-4446-49515356]

      Powder dynamics[6303234-374042-4347495052]

      Pore evolution[63133-3537-4146-474952]

      Phase transformation[634445456]

      Cracks evolution[54-55]

      Surface defect[45]

      DEDAdvanced Photon Source(APS)32-ID-B

      Ti6Al4V[57-59]

      MoNbTiV[60]

      CoCrFeMnNi[61]

      Imaging

      Powder dynamics[57]

      Melt pool dynamics[58-60]

      Pore evolution[58-60]

      Mixing of high entropy alloys during laser remelting[61]

      LPBFDeutsches Elektronen Synchrotron(DESY) PETRA ⅢHEMS-beamline P07

      CMSX-4[62-63]

      Inconel 625[63-65]

      γ-TiAl[63]

      Pure Ti[66]

      WAXS

      SAXS

      SR-XRD

      Phase transformation[62-6366]

      Stress evolution[63-66]

      Lattice spacing[6365]

      DEDDeutsches Elektronen Synchrotron(DESY) PETRA ⅢHEMS-beamline P07X40CrMoV5-1 steel[67]SR-XRD

      Microstructural evolution[67]

      Lattice parameter evolution of γ-Fe[67]

      LPBFStanford Synchrotron Radiation Laboratory(SSRL)

      2-2

      10-2

      Ti6Al4V[68-73]

      Ti5Al5V5Mo3Cr[74]

      SS316L[7072]

      Al6061[71]

      Ni400[71]

      Imaging

      SR-XRD

      Melt pool dynamics[687072-74]

      Pore evolution[6870-74]

      Lattice dynamics[68-69]

      Phase transformation[68-6974]

      Stress evolution[69]

      LPBFSwiss Light Source(SLS)MicroXAS & MS TOMCAT

      Ti6Al4V[75-76]

      CM247LC[77]

      AlSc(Zr)[78]

      Imaging

      SR-XRD

      Phase transformation[75-7678]

      Stress evolution[76]

      Cracks evolution[77]

      DEDCornell High Energy Synchrotron SourceID3A

      Inconel 625[79]

      SS304[79]

      Imaging

      SR-XRD

      Lattice strain[79]
    • Table 2. Partial application of characterization methods based on neutron diffraction in additive manufacturing

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      Table 2. Partial application of characterization methods based on neutron diffraction in additive manufacturing

      TechniqueFacilityMaterialDetectorStudy field
      LPBFJ-PARCAlSi3.5Mg2.5[80]TAKUMIExplore evolution of phase stresses, dislocation density,and crystallite size[80]
      LPBFOak Ridge National Laboratory(ORNL)Inconel 625[81]304L stainless steel[82]VULCAN engineering materials diffractometer[81-82]Time-of-flight neutron diffraction instrument[81]Measures residual stresses[81]Characterizes crystallographic texture[82]
      LPBFThe Australian Nuclear Science and Technology Organization(ANSTO)Inconel 718[83]KOWARI engineering diffractometerMeasures residual stresses[83]Visualize and quantify the distribution of internal defects and macro-porosities[83]
      LPBFISIS316L stainless steel[84]ENGIN-XRevealed mechanical and microstructural responses[84]
      LPBFNIST’s CNRStainless steel 174 PH[85]BT8 residual stress diffractometer Ordela 1150 position sensitive neutron detectorMeasures internal residual stresses Measures lattice strains[85]
      LPBFThe Australian Nuclear Science and Technology Organization(ANSTO)Ti-6Al-4V[86]KOWARI-strain scannerMeasures residual stresses[86]
      LPBFHelmholtz-Zentrum für Materialien und Energie, Berlin (HZB)Inconel 718[87]2D detectorMeasures residual stresses[87]
      Cold spray additive manufacturing(CSAM)ANSTOTi/Fe coated sample[88]KOWARIMeasures residual stresses[88]
      WAAMANSTOTiAl[89]KOWARIMeasures residual stresses[89]
      WAAMISISInconel 718[90]GEMMeasures texture[90]
      WAAMISISTi-6Al-4V[91]ENGIN_XMeasures residual stresses[91]
      DEDJ-PARCCoCrNi[92]TAKUMIMeasures lattice strain[92]
      DEDOak Ridge National Laboratory(ORNL)Inconel 625[93-95]VULCAN engineering materials diffractometerMeasures residual stresses[93-94]Characterizes crystallographic texture[95]
      DEDISISNickel-base super alloy C263[96]ENGIN_XMeasures residual elastic strain and crystallographic[96]
      EBMOak Ridge National Laboratory(ORNL)Inconel 718[97-98]VULCAN engineering materials diffractometerMeasures crystallographic texture[98]Measures peak positions of individual planes and lattice strains[97]
      EBMNational Institute of Standards and Technology(NIST)Ti-6Al-4V[99]BT8 residual stress diffractometerMeasures residual stresses[99]
      EBMCanadian Neutron Beam CenterTi-6Al-4V[100]L3 diffractometerMeasures thermal residual stress[100]
      Direct metal laser sintering(DMLS)Los Alamos Neutron Science Center(LANSCE)GP1 stainless steel[101]HIPPO instrumentMeasures texture[101]
      Direct metal laser sintering(DMLS)Canadian Nuclear Laboratories316L stainless steel[102]L3 diffractometerMeasures residual stresses[102]
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    Hongwen Deng, yi Zhang, Aodong Quan, Yudai Wang, Haibo Tang, Xu Cheng. Application of Synchrotron Radiation and Neutron Diffraction Technologies in Additive Manufacturing[J]. Chinese Journal of Lasers, 2022, 49(19): 1902002

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    Paper Information

    Category: laser manufacturing

    Received: Jul. 5, 2022

    Accepted: Sep. 13, 2022

    Published Online: Oct. 12, 2022

    The Author Email: Cheng Xu (chengxu@buaa.edu.cn)

    DOI:10.3788/CJL202249.1902002

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