Acta Optica Sinica, Volume. 42, Issue 11, 1134008(2022)

X-Ray Crystal Diffraction Spectrometer: Theory and Application

Miao Li1, Tong Yao1, Xi Wang1, Jun Shi2、*, Feng Wang3, Guohong Yang3, Wanli Shang3, Minxi Wei3, and Ao Sun3
Author Affiliations
  • 1College of Optoelectronic Engineering, Chongqing University of Posts and Telecommunications, Chongqing 400065, China
  • 2Key Laboratory of Optoelectronic Technology & Systems, Ministry of Education, Chongqing University, Chongqing 400044, China;
  • 3Laser Fusion Research Center, China Academy of Engineering Physics, Mianyang 621900, Sichuan, China
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    Figures & Tables(20)
    Schematic diagram of the Darwin differential method
    Multi-Lamellar approximate dynamic diffraction calculation model[35]. (a) Bragg crystal; (b) Laue crystal
    Correction results of rocking curves of different crystals by multilayer approximate model[37]. (a) 228.6 mm; (b) 152.4 mm; (c) 101.6 mm; (d) 50.8 mm
    Dynamic diffraction of Si(004) crystal with a 12-keV planewave[47]. (a) Simulated optical path model; (b) diffracted wave; (c) transmitted wave; (d) energy flow; (e) diffracted intensity; (f) diffracted wave in 0° deviation angle; (g) transmitted wave in 0° deviation angle; (h) energy flow in 0°deviation angle
    Structure of typical bending focusing X-ray crystal spectrometer. (a) Johann spectrometer; (b) Johansson spectrometer
    Optical path of spherical curved crystal. (a) Diffraction light path along meridional/sagittal plane; (b) focus distance of meridional/sagittal plane
    Johann spectrometer with spherical bent crystal[68]. (a) Schematic of spectrometer; (b) K-edge spectra and reference spectrum of selenium accumulation in pseudomonas
    Vacuum-formed bent crystal analyzer[70]. (a) Experimental setup; (b) focus imaging contrast of SBCA & VF-BCA
    Focusing principle of toroidal crystal. (a) Diffractive light path along meridional/sagittal plane; (b) focus distance of meridional/sagittal plane
    Toroidal spectrometer[76]. (a) Illustration of spectrometer; (b) grid imaging distribution; (c) comparison between toroidal crystal and spherical curved crystal; (d) imaging resolution
    Four-channel toroidal curved crystal spectrometer[77]
    Different von Hamos curved crystal spectrometers[78]. (a) Standard von Hamos focusing structure; (b) von Hamos focusing structure in XES spectrometer; (c) von Hamos focusing structure in XAFS spectrometer
    Comparison between von Hamos LiNbO3(014-) crystal spectrometer and Johansson Si(111) crystal spectrometer[81]. (a) Schematic of spectrometer; (b) comparison of the sulfur Kα XES
    Integrated von Hamos multi-crystal spectrometer[82]. (a) Spectrometer with sixteen Si(111) crystals; (b) spectra of elastic scattering measurement
    Segmented von Hamos spectrometer and the spectrum specifications[83]. (a) Diagram of principle; (b) diagram of setup; (c) measured Bragg angle; (d) measured resolution
    X-ray dispersion on the meridional plane of conical crystal
    Segmented conical analyzer[90]. (a) Schematic of structure; (b) measured Mn Kα lines
    Diffraction focusing structure of conical crystal spectrometer with continuous variable curvature[94]
    Variable curvature surface crystals prepared by thermoplastic method[92]. (a) Schematic of fabrication process; (b) Ge crystal with variable curvature surface; (c) acquired XRF data
    Schematic of the multi-cone crystal and its performance[96]. (a) Multi-cone α-quartz crystal; (b) spectrum comparison between multi-cone crystal and plane crystal; (c) focusing performance comparison between multi-cone crystal and plane crystal
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    Miao Li, Tong Yao, Xi Wang, Jun Shi, Feng Wang, Guohong Yang, Wanli Shang, Minxi Wei, Ao Sun. X-Ray Crystal Diffraction Spectrometer: Theory and Application[J]. Acta Optica Sinica, 2022, 42(11): 1134008

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    Paper Information

    Category: X-Ray Optics

    Received: Jan. 27, 2022

    Accepted: Mar. 3, 2022

    Published Online: Jun. 3, 2022

    The Author Email: Jun Shi (shijun@cqu.edu.cn)

    DOI:10.3788/AOS202242.1134008

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