Chinese Journal of Lasers, Volume. 51, Issue 20, 2002302(2024)

Microstructure Mechanism of Stray Grain Formation During Directed Energy Deposition of DD6 Single Crystal Superalloys

Yan Zeng1,2,3, Jingyi Guo1,2, Zheming Fan1,3, Kaichi Xu1,2, and Lei Li1,2、*
Author Affiliations
  • 1School of Mechanics, Civil Engineering and Architecture, Northwestern Polytechnical University, Xi'an 710129, Shaanxi , China
  • 2United Innovation Center of Reliability of Structure Life for Commercial Aero Engine, Xi'an 710129, Shaanxi , China
  • 3Shenzhen Research Institute, Northwestern Polytechnical University, Shenzhen 518057, Guangdong , China
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    Figures & Tables(16)
    Macroscopic morphologies of DD6 single crystal alloys. (a) Single-channel single-layer deposition; (b) single-channel 5-layer deposition
    Dendrite morphologies in single-channel single-layer deposition area. (a) Schematic of area positions; (b) bottom area; (c) middle area; (d) CET area at top
    Orientation distribution and KAM plot of DD6 single crystal alloy after single-channel 5-layer deposition. (a) Orientation distribution; (b) KAM plot
    Dendrite morphologies in I‒III regions and corresponding local orientation distributions. (a) Dendrite morphologies; (b) local orientation distributions
    Schematic of Vickers hardness test points of DD6 single crystal alloy after directed energy deposition and hardness values.(a) Schematic of test points; (b) hardness values
    Typical microscopic morphology in CET region at top. (a) Microscopic topography; (b) partial enlargement
    Thermophysical property parameters and phase diagram. (a) Thermal conductivity; (b) specific heat capacity;(c) viscosity coefficient; (d) phase diagram
    Thermal history simulation during single-channel 5-layer deposition of DD6 single crystal alloys. (a) Sweep strategy, finite element model, and selection positions of measured points during single-channel 5-layer deposition; (b) temperature changes at seven measured points during deposition process; (c) temperature gradient changes at seven measured points during deposition process
    Formation mechanism of γ/γ′ eutectic band in CET area
    Contents of different elements in γ/γ' eutectic band and dendrite core. (a) Line scanning directions; (b) line scanning result of element W; (c) line scanning result of element Re; (d) line scanning result of element Mo
    Effects of heat flow inside molten pool on element distribution and eutectic coarsening. (a) Temperature gradient and convection morphology of molten pool during deposition of DD6 single crystal alloy; (b) element content; (c) directional coarsening of γ/γ 'eutectic due to chemical gradient
    Microscopic morphologies of CET area in central area. (a) Fusion zone between dendrite core and interdendrite; (b) dendrite core area; (c) interdendrite area
    • Table 1. Chemical compositions of materials (mass fraction,%)

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      Table 1. Chemical compositions of materials (mass fraction,%)

      ElementCrCoMoWTaReAlHfNi
      Substrate4.39.02.08.07.52.05.60.1Bal.
      DD6 powder4.09.02.08.07.02.05.70.1Bal.
    • Table 2. Process parameters of DED

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      Table 2. Process parameters of DED

      Laser power /WScanning velocity /(mm/s)Beam radius /mmZ axis increment /mmPowder feed rate /(g/min)
      800‒1000100.50.4‒0.58.5‒9.5
    • Table 3. Thermophysical property parameters of materials

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      Table 3. Thermophysical property parameters of materials

      ParameterValue of CMSX-4 in referenceCalculated value of CMSX-4 by JmatproCalculated value of DD6 by Jmatpro
      Solidus temperature Ts /K16552816161608
      Liquidus temperature Tl /K16802816761658
      Density ρ /(kg/m3) (1773 K)76462876007720
      Latent heat of fusion L /(kJ/kg)231528
    • Table 4. Parameters of heat conduction model

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      Table 4. Parameters of heat conduction model

      ParameterValue
      Beam radius /mm0.5
      Absorptivity0.229
      Ambient temperature /K293.15
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    Yan Zeng, Jingyi Guo, Zheming Fan, Kaichi Xu, Lei Li. Microstructure Mechanism of Stray Grain Formation During Directed Energy Deposition of DD6 Single Crystal Superalloys[J]. Chinese Journal of Lasers, 2024, 51(20): 2002302

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    Paper Information

    Category: Laser Additive Manufacturing

    Received: Feb. 26, 2024

    Accepted: Apr. 1, 2024

    Published Online: Oct. 12, 2024

    The Author Email: Lei Li (lileinpu@nwpu.edu.cn)

    DOI:10.3788/CJL240623

    CSTR:32183.14.CJL240623

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