NUCLEAR TECHNIQUES, Volume. 48, Issue 7, 070006(2025)
Research progress on environmental compatibility evaluation in liquid lead bismuth eutectic of stainless steels used in lead-cooled fast reactor
Fig. 1. Solubility curves of metal elements in liquid lead bismuth eutectic (LBE)[1] (color online)
Fig. 2. Gibbs free energy-temperature diagram of oxides for steel exposed to liquid LBE (color online)
Fig. 3. Cross-section morphologies of typical oxide films on T91 steel under different oxygen concentrations after 1 000 h exposure in liquid LBE at 550 oC[13](a) Saturated oxygen, (b) 1.26×10-6%, (c) 1.41×10-8%, (d) 1.12×10-9%
Fig. 4. Cross section morphologies of 9Cr ferritic/martensitic steel after exposed to 10-6% oxygen-controlled LBE at 600 ℃[31](a) 1.0Si (1 000 h), (b) 0Si (2 000 h), (c) 0.7Si (2 000 h), (d) 1.0Si (2 000 h)
Fig. 7. (a) SEM-BSE image and EDS elemental distributions of the oxide scale on the 2 000 h exposure 316L specimen, (b, c) the corresponding BC and IPF maps at a specimen tilt of 70°[63]
Fig. 8. APT analysis of the dual-phase structure in inner oxide layer of Si-enhanced stainless steel after exposure to oxygen-saturated LBE for 1 000 h[70] (color online)(a) BSE image showing the location of APT samples, (b, c) BSE and SEM image of APT needle-like sample, (d) O, Ni, and Si atoms mappings, and (e) the proximity histogram across the interface of Fe-Cr spinel/(Fe, Ni)-rich phase based on an iso-concentration surface of about 22% (atomic percentage) Ni in Fig.(d)
Fig. 9. HAADF-STEM image and corresponding EDS elemental distributions of cross section in 14Ni steel after exposed in LBE (1.8 m∙s-1, 5×10-7%~5×10-6%) at 550 ℃ for 4 008 h[77] (color online)
Fig. 10. Correlation of fatigue lives of 316LN SS with strain amplitude in liquid LBE and in air at 400 ℃[86]
Fig. 12. (a, b) HAADF images of the segregation-induced ordered Pb/Bi-Fe superstructures and Pb-Bi clusters discontinuously distributed at the GB1 and GB2 at 350 ℃, (c) High magnification HAADF image at GB1, (d) Atomic super EDS mappings in Fig.(c)[59] (color online)
Fig. 13. STEM observation of the grain boundary and Pb-Bi precipitates ahead of the crack tip for 316LN AuSS fatigue crack propagation tested at 400 ℃ of liquid LBE[90] (color online) (a) HAADF images of the Pb-Bi precipitate at the grain boundary, (b, c) Interfacial cracking along twin boudaries, (d) Phase identification of the Pb-Bi cluster, (e, f) The Pb-Bi particle was embedded at twin boudaries
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Jibo TAN, Xinrui ZHANG, Baoquan XUE, Ziyu ZHANG, Xinqiang WU. Research progress on environmental compatibility evaluation in liquid lead bismuth eutectic of stainless steels used in lead-cooled fast reactor[J]. NUCLEAR TECHNIQUES, 2025, 48(7): 070006
Category: Special Issue on The First Academic Annual Conference of the Research Reactor and Innovative Reactor Association of Chinese Nuclear Society and Advanced Nuclear Power System Reactor Engineering
Received: Apr. 19, 2025
Accepted: --
Published Online: Sep. 15, 2025
The Author Email: Xinqiang WU (WUXinqiang)