Acta Optica Sinica, Volume. 42, Issue 10, 1031001(2022)

Anti-Reflection Surface of Mid-Infrared Bionic Composite Micro-Nano Structure

Ziye Ma, Mingzhao Ouyang*, Yuegang Fu, Jinshuang Wu, Jianhong Zhou, Hang Ren, and Ziqiang Zhang
Author Affiliations
  • Key Laboratory of Optical Control and Optical Information Transmission Technology, Ministry of Education, Changchun University of Science and Technology, Changchun 130022, Jilin, China
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    Figures & Tables(9)
    Experimental process
    SEM images. (a) SEM image of PS microsphere mask; (b) side view of moth eye structure on silicon wafer after ICP etching; (c) top view of Al2O3-Si structure; (d) side view of Al2O3-Si structure
    Results of spectral reflectance tests. (a) Actually measured reflectance of structure surface with different Al2O3 film thickness; (b) average reflectance for different Al2O3 film thickness
    Comparison of test and simulation reflectance of single structure and composite structure at 8° incidence angle
    Reflectance of single micro-nano structure surface and composite micro-nano structure surface (Al2O3 thickness of 185 nm) for P-polarization and S-polarization at incidence angle for 8°. (a) Single micro-nano structure; (b) composite micro-nano structure
    Electric field distributions of Al2O3-Si structure under different Al2O3 thicknesses. (a) Al2O3 (0 nm); (b) Al2O3 (100 nm); (c) Al2O3 (150 nm); (d) Al2O3 (185 nm)
    P-h curves of single structure and composite micro-nano structure samples obtained by different treatment methods
    • Table 1. Process parameters for preparation of Al2O3 based on ALD technology

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      Table 1. Process parameters for preparation of Al2O3 based on ALD technology

      ConditionMaterialSubstratetemperature /℃First reactant(pulse time)Purge gas(purge time)Second reactant(pulse time)Purge gas(purge time)
      DetailAl2O3200TMA (0.02 s)Ar (8 s)H2O (0.02 s)Ar(8 s)
    • Table 2. Elastic recovery rate

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      Table 2. Elastic recovery rate

      SampleDisplacementat max loadhmax /nmResidualpressuredepth hr /nmElasticrecoveryrate φ /%
      Moth-eye+HF+Al2O3253.423193.691023.57
      Moth-eye+Al2O3256.605206.103419.68
      Moth-eye320.418277.400013.43
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    Ziye Ma, Mingzhao Ouyang, Yuegang Fu, Jinshuang Wu, Jianhong Zhou, Hang Ren, Ziqiang Zhang. Anti-Reflection Surface of Mid-Infrared Bionic Composite Micro-Nano Structure[J]. Acta Optica Sinica, 2022, 42(10): 1031001

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    Paper Information

    Category: Thin Films

    Received: Sep. 28, 2021

    Accepted: Dec. 6, 2021

    Published Online: May. 10, 2022

    The Author Email: Ouyang Mingzhao (oymz68@163.com)

    DOI:10.3788/AOS202242.1031001

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