Laser & Optoelectronics Progress, Volume. 59, Issue 19, 1931003(2022)

High Crystallization Quality β-Ga2O3 Films Prepared by Chemical Vapor Deposition

Xingchen Li, Fengyuan Lin*, Huimin Jia, Yubin Kang, Yongji Shi, Bingheng Meng, Dan Fang, Jilong Tang, Dengkui Wang, Kexue Li, Xueying Chu, and Zhipeng Wei
Author Affiliations
  • State Key Laboratory of High Power Seminconductor Laser, College of Science, Changchun University of Science and Technology, Changchun130022, Jinlin, China
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    Figures & Tables(8)
    Schematic diagram of CVD growth system and temperature distribution. (a) CVD growth system; (b) temperature distribution
    CVD epitaxial growth procedure
    Characterization of the Ga2O3 films grown under different carrier gases at a growth temperature of 650 ℃ and a growth time of 30 min. (a) XRD pattern; (b) Raman spectroscopy
    XRD pattern of Ga2O3 films at different growth temperatures. (a) (b) XRD pattern of samples grown at different temperatures; (c) AFM image of the film grown at 750 ℃; (d) SEM image of the film grown at 750 ℃; (e) height map of the films grown at 750 ℃
    Characterization of samples at different growth times, under the conditions of growth temperature of 750 ℃ and Ar as carrier gas. (a) XRD pattern of β-Ga2O3 films grown under different growth times; (b) AFM image of the β-Ga2O3 film grown at a growth time of 20 min
    • Table 1. Growth conditions of sample 1 and sample 2

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      Table 1. Growth conditions of sample 1 and sample 2

      Sample numberBuffer gasGrowth time /minTemperature /℃Oxygen flow rate /(mL·min-1
      Sample 1Ar306501
      Sample 2N2306501
    • Table 2. Growth conditions of samples 3 to 8

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      Table 2. Growth conditions of samples 3 to 8

      Sample numberBuffer gasGrowth time /minTemperature /℃Oxygen flow rate /(mL·min-1
      Sample 3Ar206501
      Sample 4Ar207301
      Sample 5Ar207401
      Sample 6Ar207501
      Sample 7Ar207601
      Sample 8Ar208501
    • Table 3. Growth conditions of sample 9, 6, and 1

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      Table 3. Growth conditions of sample 9, 6, and 1

      Sample numberBuffer gasGrowth time /minTemperature /℃Oxygen Flow Rate /(mL·min-1
      Sample 9Ar107501
      Sample 6Ar207501
      Sample 1Ar307501
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    Xingchen Li, Fengyuan Lin, Huimin Jia, Yubin Kang, Yongji Shi, Bingheng Meng, Dan Fang, Jilong Tang, Dengkui Wang, Kexue Li, Xueying Chu, Zhipeng Wei. High Crystallization Quality β-Ga2O3 Films Prepared by Chemical Vapor Deposition[J]. Laser & Optoelectronics Progress, 2022, 59(19): 1931003

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    Paper Information

    Category: Thin Films

    Received: Sep. 6, 2021

    Accepted: Oct. 11, 2021

    Published Online: Oct. 11, 2022

    The Author Email: Lin Fengyuan (linfengyuan_0116@163.com)

    DOI:10.3788/LOP202259.1931003

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