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Chinese Journal of Lasers, Volume. 48, Issue 7, 0703001(2021)

Surface Treatment of Fluorozirconate Glass Fiber Preform Using Nonaqueous Solution

Huiyu Chen1,2, Xin Wang1, Tianfeng Xue1, Tao Meng1, Hong He1, Meisong Liao1, Lili Hu1, and Wei Chen1、*
Author Affiliations
  • 1Shanghai Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, Shanghai 201800
  • 2University of the Chinese Academy of Sciences, Beijing 100049
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    AbstractGet PDF(in Chinese)
    Figures&Tables (8)
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    Figures & Tables(8)
    Structure model of glass surface[27]

    Fig. 1. Structure model of glass surface[27]

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    Surface compositions of fluorozirconate glass treated by different surface treatments

    Fig. 2. Surface compositions of fluorozirconate glass treated by different surface treatments

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    Surface roughness of sample after treatment by method a

    Fig. 3. Surface roughness of sample after treatment by method a

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    Surface roughness of sample after treatment by method c

    Fig. 4. Surface roughness of sample after treatment by method c

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    Surface roughness of sample after treatment by method b

    Fig. 5. Surface roughness of sample after treatment by method b

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    Optical loss of fluorozirconate glass fibres drawn from preforms after surface treatments with different solutions

    Fig. 6. Optical loss of fluorozirconate glass fibres drawn from preforms after surface treatments with different solutions

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    Fracture probabilities of fluorozirconate glass fibres drawn from preforms after surface treatments with different solutions

    Fig. 7. Fracture probabilities of fluorozirconate glass fibres drawn from preforms after surface treatments with different solutions

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    • Table 1. Compositions and proportions of two surface treating agents

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      Table 1. Compositions and proportions of two surface treating agents

      Surface treatment agentSolventAcidAdditive
      Non-aqueous organicsolutionEthyl alcohol with mass fraction of 70%+amyl alcohol with mass fraction of 15%Hydrochloric acid with mass fraction of 4%+oxalic acid with mass fraction of 6%Zirconyl chloride with mass fraction of 3%+ethylene diamine tetraacetic acid with mass fraction of 2%
      Aqueous containingsolutionDeionized water with mass fraction of 86%Hydrochloric acid with mass fraction of 4%Zirconyl chloride with mass fraction of 10%
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    Huiyu Chen, Xin Wang, Tianfeng Xue, Tao Meng, Hong He, Meisong Liao, Lili Hu, Wei Chen. Surface Treatment of Fluorozirconate Glass Fiber Preform Using Nonaqueous Solution[J]. Chinese Journal of Lasers, 2021, 48(7): 0703001

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    Paper Information

    Category: materials and thin films

    Received: Jul. 31, 2020

    Accepted: Nov. 2, 2020

    Published Online: Mar. 19, 2021

    The Author Email: Chen Wei (weichen@siom.ac.cn)

    DOI:10.3788/CJL202148.0703001

    Topics

    laser devices and laser physics
    Lasers and Laser Optics
    Laser physics
    laser manufacturing
    Instrumentation, Measurement and Metrology