Acta Optica Sinica, Volume. 43, Issue 13, 1305001(2023)

Fabrication of Silicon Echelle Grating by Ultraviolet Lithography Combined with Wet Etching

Zijiang Yang1,2,3, Qiao Pan1,2,3、*, Jiacheng Zhu1,2,3, and Weimin Shen1,2,3
Author Affiliations
  • 1Key Lab of Advanced Optical Manufacturing Technologies of Jiangsu Province, Suzhou 215006, Jiangsu, China
  • 2Key Lab of Modern Optical Technologies of Education Ministry of China, Suzhou 215006, Jiangsu, China
  • 3School of Optoelectronic Science and Engineering, Soochow University, Suzhou 215006, Jiangsu, China
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    Figures & Tables(17)
    Anisotropic etching of (100) monocrystalline silicon
    Schematics of echelle grating. (a) Traditional echelle grating; (b) silicon echelle grating
    Diffraction efficiency varying with platform duty ratio f at different working orders. (a) 47; (b) 41; (c) 36
    Tolerance analysis of grating platform duty ratio
    Fabrication process of echelle gratings. (a) Substrate pre-processing; (b) oxide layer growing; (c) photoresist spinning; (d) ultraviolet exposure and development; (e) oxygen plasma etching; (f) ICP etching; (g) wet etching; (h) high-reflecting film coating
    Grating after mask collapse under optical microscope
    Schematic of over-etching after reaching the self-stopping surface
    SEM photos of silicon echelle grating with or without crystal alignment. (a) Without crystal alignment; (b) with crystal alignment
    SEM photos of 42 lp/mm silicon echelle grating. (a) Magnification of 300×; (b) magnification of 1000×
    Grating photos after coating. (a) Top view; (b) dispersion diagram
    Schematic of diffraction efficiency testing device of echelle grating
    Measurement results of diffraction efficiency at corresponding blazed wavelength of working orders
    Test results of grating sidewall surface roughness
    • Table 1. Working parameters of grating

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      Table 1. Working parameters of grating

      ParameterValue
      Wavelength /nm800-1100
      Groove density /(lp·mm-142
      Incident angle /(°)54.74
      Incident conditionQuasi Littrow mounting
      Diffraction order35-48
      Orientation angle /(°)6.4
    • Table 2. Free spectral ranges corresponding to working diffraction orders of grating

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      Table 2. Free spectral ranges corresponding to working diffraction orders of grating

      Diffraction orderFree spectral range /nm
      48796-813
      47813-830
      46830-849
      45849-868
      44868-888
      43888-909
      42909-930
      41930-953
      40953-978
      39978-1003
      381003-1030
      371030-1058
      361058-1088
      351088-1119
    • Table 3. Parameters of grating groove

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      Table 3. Parameters of grating groove

      ParameterValue
      Groove spacing /mm23.81
      Blazed angle /(°)54.74
      Groove apex angle /(°)70.52
      High-reflecting filmAg
      High-reflecting film thickness /nm150
    • Table 4. Measurement results of grating

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      Table 4. Measurement results of grating

      ParameterRequirementMeasured value
      Maximum diffraction efficiency of each working order /%>4045-55
      Groove space /μm23.81±0.2023.80
      Blazed angle /(°)54.74±0.2054.74
      Roughness of sidewall /nm0.57
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    Zijiang Yang, Qiao Pan, Jiacheng Zhu, Weimin Shen. Fabrication of Silicon Echelle Grating by Ultraviolet Lithography Combined with Wet Etching[J]. Acta Optica Sinica, 2023, 43(13): 1305001

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    Paper Information

    Category: Diffraction and Gratings

    Received: Jan. 6, 2023

    Accepted: Feb. 20, 2023

    Published Online: Jul. 12, 2023

    The Author Email: Pan Qiao (panqiao@suda.edu.cn)

    DOI:10.3788/AOS230446

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