Chinese Journal of Lasers, Volume. 49, Issue 22, 2202021(2022)

Microstructure and Mechanical Properties of High-Nitrogen Stainless Steel Manufactured by Selective Laser Melting

Lü Yuan, Tao Li, Jie Liu*, and Kehong Wang
Author Affiliations
  • Key Laboratory of Controlled Arc Intelligent Additive Manufacturing Technology, Ministry of Industry and Information Technology, Nanjing University of Science and Technology, Nanjing 210094, Jiangsu,China
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    Figures & Tables(16)
    HNS powder . (a) Morphology; (b) particle size distribution
    Schematic of SLM forming equipment
    Schematic of laser scanning direction for SLM formed metallographic specimen and tensile specimen
    Tensile test platform with high-energy synchronous X-ray
    Cross-section photos of SLM formed samples under different Ev. (a) Optical photo when Ev=190.5 J·mm-3; (b) optical photo when Ev=238.1 J·mm-3; (c) optical photo when Ev=285.7 J·mm-3 ; (d) SEM photo when Ev=238.1 J·mm-3
    Relative densities of SLM formed samples under different Ev
    XRD patterns of SLM formed samples under different Ev
    Microstructures of SLM formed samples under different Ev. (a) Ev=190.5 J·mm-3; (b) Ev=238.1 J·mm-3; (c) Ev=285.7 J·mm-3; (d) local magnification of microstructure in box area in Fig. 8(b)
    Tensile properties of samples under different Ev
    Fracture morphologies of tensile specimens formed by SLM under different Ev. (a)(d) Ev=190.5 J·mm-3; (b)(e) Ev=238.1 J·mm-3; (c)(f) Ev=285.7 J·mm-3
    Test results by high-energy X-ray synchrotron radiation. (a) Diffraction rings of specimen before tension by high-energy X-ray synchrotron radiation; (b) XRD patterns by synchrotron radiation
    Behavior of nitrogen during SLM
    • Table 1. Chemical compositions of HNS powder

      View table

      Table 1. Chemical compositions of HNS powder

      ElementMnCrMoNCSiSOFe
      Mass fraction /%10.38023.7402.8700.950<0.020<0.500<0.005<0.100Bal.
    • Table 2. Volume energy density for each set of laser parameters

      View table

      Table 2. Volume energy density for each set of laser parameters

      Serial

      number

      Laser

      power /W

      Scanning speed /(mm·s-1Ev /(J·mm-3
      1160400190.5
      2200238.1
      3240285.7
    • Table 3. Nitrogen contents of SLM formed samples under different Ev

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      Table 3. Nitrogen contents of SLM formed samples under different Ev

      Serial numberEnergy density /(J·mm-3Mass fraction of nitrogen / %
      1190.50.84
      2238.10.76
      3285.70.68
    • Table 4. FWHM and diffraction angle of SLM formed sample

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      Table 4. FWHM and diffraction angle of SLM formed sample

      Ev /(J·mm-3

      Diffraction angle of

      γ-Fe(111)/(°)

      FWHM of γ-Fe(111)

      Diffraction angle of

      α-Fe(110)/(°)

      FWHM of α-Fe(110)
      190.542.980.3144.330.32
      238.142.940.3144.300.39
      285.743.010.3844.250.52
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    Lü Yuan, Tao Li, Jie Liu, Kehong Wang. Microstructure and Mechanical Properties of High-Nitrogen Stainless Steel Manufactured by Selective Laser Melting[J]. Chinese Journal of Lasers, 2022, 49(22): 2202021

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    Paper Information

    Category: laser manufacturing

    Received: Apr. 13, 2022

    Accepted: Jun. 14, 2022

    Published Online: Nov. 10, 2022

    The Author Email: Liu Jie (j.liu@njust.edu.cn)

    DOI:10.3788/CJL202249.2202021

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