Optics and Precision Engineering, Volume. 31, Issue 15, 2227(2023)

Rapid ICP-based fabrication of large-area silicon three-dimensional interconnected honeycomb microwell array

Zhenghao LI1,2, Xiao LÜ1, Huan LI1, Long CHENG1,2, Wenchao ZHOU1、*, and Yihui WU1、*
Author Affiliations
  • 1Chinese Institute of Optics, Fine Mechanics and Physics, Chinese Academy of Sciences, Changchun30033, China
  • 2University of Chinese Academy of Sciences, Beijing100049, China
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    Figures & Tables(9)
    Top view of microwells fabricated by two-step etching(The microwells presents an equilateral triangle distribution)
    Fabrication process schematic(The etching gas SF6 reacts with silicon for etching, and the protective gas C4F8 is released to form a polymer on the surface to prevent the etching. The alternate release of protective gas and etching gas makes the sidewall tend to be vertical, and the sidewall will have a corrugated shape as observed by the local magnification, and the isotropic etching widens the internal area)
    Tilted 45° observation using SEM
    Variation of isotropic etched structure size with time observed at 45° by SEM
    Isotropic etching time versus height and width respectively
    Linear relationship between etching depth in the first step and experimentally obtained structure
    SEM images of relationship between angle of upper wall and side wall with different first etching depths
    • Table 1. Positive triangular arrangement of microwell array masks(Microwells center distance 6 micrometre,diameter 4 micrometre)

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      Table 1. Positive triangular arrangement of microwell array masks(Microwells center distance 6 micrometre,diameter 4 micrometre)

      EtchingSccm & sICP/Wt/s
      SF6C4F8
      Anisotropic500,1.5200,1.52 500/12020
      Isotropic500,1.50,02 500/12015
    • Table 2. Positive triangular arrangement of microwell array masks (Microwells center distance 8 micrometre,diameter 4 micrometre)

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      Table 2. Positive triangular arrangement of microwell array masks (Microwells center distance 8 micrometre,diameter 4 micrometre)

      EtchingSccm & sICP/Wt/s
      SF6C4F8
      Anisotropic500,1.5200,1.52 500/12025
      Isotropic500,1.50,02 500/12033
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    Zhenghao LI, Xiao LÜ, Huan LI, Long CHENG, Wenchao ZHOU, Yihui WU. Rapid ICP-based fabrication of large-area silicon three-dimensional interconnected honeycomb microwell array[J]. Optics and Precision Engineering, 2023, 31(15): 2227

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    Paper Information

    Category: Micro/Nano Technology and Fine Mechanics

    Received: Jan. 3, 2023

    Accepted: --

    Published Online: Sep. 5, 2023

    The Author Email: Wenchao ZHOU (zhouvc@ciomp.ac.cn), Yihui WU (yihuiwu@ciomp.ac.cn)

    DOI:10.37188/OPE.20233115.2227

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