Spectroscopy and Spectral Analysis, Volume. 42, Issue 1, 215(2022)
Analysis of Material and Source of Archaic Jade From the Tomb of Marquis Yi of Zeng in Suizhou, Hubei Province
Figures & Tables(7)
Fig. 1. Some archaic jade from the tomb of Marquis Yi of Zeng
(a): No soak-induced color tremolite; (b): Light soak-induced color tremolite; (c): Medium soak-induced color tremolite; (d): Severe soak-induced color tremolite; (e): Marble; (f): Mica jade; (g): Crystal; (h): Fluorite; (i): Quartzite
Fig. 2. Infrared spectra of different categories archaic jade infrared spectrogram
Fig. 3. Some samples with origin information
(a)—(d): Retaining the epidermal characteristics of gobi materials; (e)—(f): With weathered skin
Table 1. Basic gemological characteristics of archaic jades
View tableView in ArticleTable 1. Basic gemological characteristics of archaic jades
样品类别 颜色 光泽 沁色 表面受沁程度 比重 透闪石类 以白、 青白、 灰白为主, 有少量
青黄色、 青色、 青花的玉器油脂光泽-弱油脂光泽 白色、 褐色 无-重度受沁 2.80~3.10(通常2.95) 大理岩类 白色、 褐色 土状光泽 白色、 褐色 严重受沁 2.60~2.90 云母质类 青灰色、 青黄色、 浅褐色 蜡状光泽 褐黄色、 浅褐色 极轻微-轻微受沁 2.70~2.90 石英质类 褐红色 油脂光泽 未受沁 - 2.60 萤石类 灰白色 弱玻璃光泽 未受沁 - 3.16 水晶类 无色 玻璃光泽 未受沁 - 2.63~2.65
Table 2. Attribution of infrared spectrum peaks of the unearthed jade
View tableView in ArticleTable 2. Attribution of infrared spectrum peaks of the unearthed jade
材质 峰位 标准谱峰 归属指派 透闪石 1 144, 1 039, 997, 924 1 137, 1 040, 997, 921 O—Si—O, Si—O—Si的反对称伸缩振动及O—Si—O对称伸缩振动 761, 687 762, 687 Si—O—Si对称伸缩振动 510, 461, 419 538, 513, 467 Si—O的弯曲振动和M—O的晶格振动 大理岩 1 538 1 450 C—O键的不对称伸缩振动 897, 729 892, 726 C—O键的弯曲振动 云母 1 080, 1 037 1 022 Si—O—Si的伸缩振动 930, 835 935, 833, 803 Al—O-面外振动(830附近), OH的摆动(950~800) 748 754 Al—O—Si面内振动(750附近) 537, 482 533, 479, 412 Si—O的弯曲振动(530附近), OH的平移振动(520~400) 石英岩 1 180, 1 147 1 168, 1 086 Si—O—Si反对称伸缩振动 803, 785, 695, 541, 498 798, 779, 695, 515, 462 Si—O键对称伸缩振动 水晶 1 184, 1 147 1 170, 1 085 Si—O—Si反对称伸缩振动 804, 786, 696, 543, 498 798, 779, 695, 519, 462 Si—O键对称伸缩振动
Table 3. Main chemical components of some archaic jade samples
View tableView in ArticleTable 3. Main chemical components of some archaic jade samples
编号 SiO2/% MgO/% CaO/% FeO/% Al/10-6 Mn/10-6 Na/10-6 K/10-6 Ti/10-6 Mg/Mg+Fe E.243 58.2 22.6 16.3 2.0 4 344 1 651 745 1 051 56 0.92 透闪石 W.C.7: 7 59.4 24.2 15.3 0.7 2 738 302 607 672 138 0.97 E.48 58.7 25.2 14.8 0.9 3 020 768 694 211 17 0.97 编号 SiO2/% MgO/% CaO/% FeO/% Al2O3/% Mn/10-6 Na/10-6 K/10-6 Ti/10-6 CaO:MgO E.75-13 1.6 15.7 38.7 0.1 1.375 209 780 623 207 2.46 大理岩 N.344-2 1.7 16.2 38.1 0.1 1.720 171 639 917 210 2.35 W.C.6:3 2.1 15.2 38.7 0.1 0.916 113 341 1097 246 2.54 编号 SiO2/% MgO/% CaO/% FeO/% Al2O3/% K2O/% Mn/10-6 Na/10-6 Ti/10-6 P/10-6 N.341 62.7 3.7 2.2 1.9 8.6 15.9 1 020 1 292 966 779 云母质 W.C.2:6 78.5 2.3 0.9 0.5 4.4 5.3 99 834 3 825 544 E.C.8:6 61.2 3.3 0.2 4.2 8.8 14.5 342 1 110 1 813 276 编号 SiO2/% MgO/% CaO/% FeO/% Al/10-6 Mn/10-6 Na/10-6 K/10-6 Ti/10-6 P/10-6 石英岩 E.C.11:266 96.4 2.1 0.3 0.4 3 283 62 665 2 563 1 003 1 353 编号 SiO2/% MgO/% CaO/% FeO/% Al/10-6 Mn/10-6 Na/10-6 K/10-6 Ti/10-6 萤石 N.361 1.0 0.7 97.9 0.1 1 116 32 271 1 141 307 编号 SiO2/% MgO/% CaO/% FeO/% Al/10-6 Mn/10-6 Na/10-6 K/10-6 Ti/10-6 P/10-6 水晶 E.C.2:7 98.5 1.3 0.0 0.0 1 880 11 436 59 3 254
Table 4. The excavated location, material and quantity statistics of the test samples
View tableView in ArticleTable 4. The excavated location, material and quantity statistics of the test samples
出土位置 材质 数量 东室 东室主内棺 透闪石质玉 175 石英岩 1 东室主外棺 透闪石质玉 8 东室外棺内底西侧 透闪石质玉 3 东室陪葬棺 透闪石质玉 16 云母质玉 1 水晶 2 东室殉狗棺 大理岩 2 东室 透闪石质玉 22 云母质玉 1 大理岩 34 东壁外采集 透闪石质玉 1 西室 西室陪葬棺 透闪石质玉 34 云母质玉 5 大理岩 3 西室椁室内 透闪石质玉 2 西室 透闪石质玉 1 北室 透闪石质玉 2 云母质玉 1 大理岩 4 萤石 1
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Ji-fu LIU, Ming-xing YANG, Yue SU, Yue LIU. Analysis of Material and Source of Archaic Jade From the Tomb of Marquis Yi of Zeng in Suizhou, Hubei Province[J]. Spectroscopy and Spectral Analysis, 2022, 42(1): 215
Paper Information
Category: Research Articles
Received: Nov. 11, 2020
Accepted: --
Published Online: Mar. 31, 2022
The Author Email: Ji-fu LIU (liujf@cug.edu.cn)
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