Design on the Comprehensive Experiment for the Green Oximation Reaction

Shiming FAN; Wei YU; Aoqi LI; Sifan DONG; Tianjiao HAN

doi:10.12179/1672-4550.20220452

Experiment Science and Technology, Volume. 22, Issue 2, 76(2024)

Design on the Comprehensive Experiment for the Green Oximation Reaction

Shiming FAN¹, Wei YU², Aoqi LI¹, Sifan DONG¹, and Tianjiao HAN^3、*

¹State Key Laboratory Breeding Base-Hebei Province Key Laboratory of Molecular Chemistry for Drug, Hebei University of Science and Technology, Shijiazhuang 050018, China

²R & D Center, Hebei Grand Jiufu Biotechnology Co., Ltd., Baoding 072150, China

³New Preparation Branch Factory, North China Pharmaceutical Co., Ltd., Shijiazhuang 050000, China

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Figures & Tables(9)

Fig. 1.

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Fig. 6.

Table 1. [in Chinese]
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Table 1. [in Chinese]
编号溶剂时间/h 平均粒径/nm
1 月桂酸/乙醇 0 53000
2 月桂酸/乙醇 1 893
3 月桂酸/乙醇 2 364
4 月桂酸/乙醇 3 95
5 月桂酸/乙醇 4 64
6 月桂酸/乙醇 5 64
7 乙醇 4 266

Table 2. [in Chinese]
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Table 2. [in Chinese]
对比物 α峰 β峰总碱度
Nano-K₂CO₃ 0.385 0.032 0.417
Normal-K₂CO₃ 0.105 0.105

Table 3. [in Chinese]
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Table 3. [in Chinese]
平均粒径/nm 收率/%
53000 13.1
893 32.1
364 67.3
95 89.1
64 94.5

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Shiming FAN, Wei YU, Aoqi LI, Sifan DONG, Tianjiao HAN. Design on the Comprehensive Experiment for the Green Oximation Reaction[J]. Experiment Science and Technology, 2024, 22(2): 76

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