NUCLEAR TECHNIQUES, Volume. 47, Issue 4, 040203(2024)
Exploring the defects evolution of nuclear graphite by using micro-Raman characterization on the cross-section of 107Ag5+ ion irradiated nuclear graphite at high temperature
Fig. 1. Schematic diagram of sample irradiation and cross-sectional micro-Raman spectroscopy(a) The micro-Raman device, (b) Two-dimensional Raman spectroscopy physics and pixel size (color online)
Fig. 2. Energy loss of 30 MeV 58Ni5+ and 107Ag5+ ions in graphite carbon (ICRU-906) target calculated by using the all-cascade damage model, the vacancies and ion distributions generated by the two types of ions(a) Electron energy loss, (b) Nuclear energy loss, (c) Total energy loss, (d) 58Ni5+, (e) 107Ag5+
Fig. 3. Normalized Raman spectra of nuclear graphite irradiated by 107Ag5+ ions as a function of different depths: the line scan graph (a) and typical Raman spectra at different depths (c) under dose of 0.3×1016 ions∙cm-2; the line scan graph (b) and typical Raman spectra at different depths (d) under dose of 0.9×1016 ions∙cm-2 (color online)
Fig. 4. Schematic diagram of the Raman spectra fitting for nuclear graphite (color online)(a) Pristine nuclear graphite, (b) Irradiated nuclear graphite
Fig. 5. Grayscale map of different Raman parameters for the D peak and G peak under different doses of 0.3×1016 ions∙cm-2 (a~h) and 0.9×1016 ions∙cm-2 (a1~h1): (a, a1) D Position, (b, b1) D area, (c, c1) FWHM(D), (d, d1) D height, (e, e1) G position, (f, f1) G area, (g, g1) FWHM(G), (h, h1) G height
Fig. 6. Comparison of ID/IG at different depths of nuclear graphite irradiated by 107Ag5+ ions with different fluences: the grayscale map (a) and scatter plots (c) under dose of 0.3×1016 ions∙cm-2; the grayscale map (b) and scatter plots (d) under dose of 0.9×1016 ions∙cm-2
Fig. 7. Variation of the G peak position of nuclear graphite and comparison of Raman spectra between heavily irradiated regions and unirradiated regions under irradiation fluence of 0.3×1016 ions∙cm-2 (a) and 0.9×1016 ions∙cm-2 (b); Standard error plots of G peak at different depths under irradiation fluence of 0.3×1016 ions∙cm-2 (c) and 0.9×1016 ions∙cm-2 (d)
Fig. 8. Scatter plot showing the variation of Raman spectral characteristic parameters of IG-110 irradiated with 107Ag5+ and 58Ni5+[23] ions as a function of DPA (a) ID/IG , (b) FWHM(G)
Fig. 9. ID/IGvs. FWHM(G) for irradiated regions (solid symbols) and unirradiated regions (hollow symbols) under different ion irradiations (color online)
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Yiyan LI, Zhoutong HE, Xiuliang ZHAO, Shancheng PENG, Huilei MA. Exploring the defects evolution of nuclear graphite by using micro-Raman characterization on the cross-section of 107Ag5+ ion irradiated nuclear graphite at high temperature[J]. NUCLEAR TECHNIQUES, 2024, 47(4): 040203
Category: Research Articles
Received: Feb. 22, 2024
Accepted: --
Published Online: May. 28, 2024
The Author Email: Xiuliang ZHAO (赵修良)