Chinese Journal of Lasers, Volume. 49, Issue 8, 0802009(2022)

Effect of Different Heat Treatments on Microstructure, Properties, and Anisotropy of SLM TC4

Zhen Dou1, Yuyue Wang1, Anfeng Zhang2、*, Mengjie Wu2, and Puqiang Wang1
Author Affiliations
  • 1State Key Laboratory for Mechanical Behavior of Materials, Xi'an Jiaotong University, Xi'an 710049, Shaanxi, China
  • 2State Key Laboratory for Manufacturing Systems Engineering, Xi'an Jiaotong University, Xi'an 710054, Shaanxi, China
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    Figures & Tables(11)
    Schematic diagram of SLM TC4 sample forming method and size. (a) Schematic of horizontal specimen;(b) schematic of vertical specimen; (c) physical drawing of horizontal forming; (d) physical drawing of vertical forming
    Macro morphology of SLM TC4. (a) SLM-V; (b) SLM-H
    Images of low-magnification microstructure of SLM TC4 deposited state and different heat treatment processes. (a) As-deposited; (b) HM1; (c) HM2; (d) HM3
    SEM images of low-magnification microstructure of SLM TC4 deposited state and different heat treatment processes. (a) As-deposited; (b) HM1; (c) HM2; (d) HM3
    Anisotropic histogram of microstructure in deposited state and different heat treatment processes
    Tensile stress state of grain boundaries in different directions and crack propagation path diagram. (a) SLM-H;(b) SLM-V; (c) schematic diagram of crack propagation pathin deposited state and after heat treatment
    Tensile fracture morphology of SLM TC4 in deposited state. (a) SLM-H(×80); (b) SLM-H(×2000); (c) SLM-H(×5000); (d) SLM-V (×80); (e) SLM-V(×2000); (f) SLM-V(×5000)
    Topography of the tensile fracture of different heat treatment processes. (a) HM1-H(×80); (b) HM1-H(×2000); (c) HM1-V(×80); (d) HM1-V(×2000); (e) HM2-H(×80); (f) HM2-H(×2000); (g) HM2-V(×80); (h) HM2-V(×2000); (i) HM3-H(×80); (j) HM3-H(×2000); (k) HM3-V(×80); (l) HM3-V(×2000)
    • Table 1. Chemical composition of TC4 powder

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      Table 1. Chemical composition of TC4 powder

      ElementAlVFeCNHOTi
      Mass fraction /%6.013.920.1640.0050.0020.0010.072Bal.
    • Table 2. Heat treatment processes of SLM TC4 alloy

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      Table 2. Heat treatment processes of SLM TC4 alloy

      No.Heat treatment processes
      SLMAs-built
      HM1TC4 samples are first air cooled after solution treatment at 950 ℃ for 1 h, and then air is cooled after aging at 550 ℃ for 4 h.
      HM2TC4 samples are heated to 920 ℃ for 5 min, then cooled to 700 ℃ for 10 min in the furnace, which is repeated five times and then samples are air cooled.
      HM3TC4 samples are kept at 920 ℃ for 10 min, cooled slowly to 800 ℃ and kept for 30 min in the furnace. When the temperature is 550 ℃,samples are immediately heated to 920 ℃. The whole process is repeated for 4 times and then samples are cooled in the furnace. At last the solution heat treating is performed at 920 ℃ for 1 h and aging treatment is performed at 550 ℃ for 4 h.
    • Table 3. Mechanical properties of SLM TC4 alloy tensile specimens under different treatment conditions

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      Table 3. Mechanical properties of SLM TC4 alloy tensile specimens under different treatment conditions

      TreatmentTensile directionUltimate tensile strength σb/MPaYield strength σs/MPaElongation /%Rate of reduction in area /%
      SLMH1226.0±19.541048.2±19.1513.1±1.1642.6±1.85
      V1220.0±8.081060.2±8.2111.5±1.8240.2±2.32
      HM1H952.4±3.61862.4±3.2617.5±1.7949.2±1.17
      V963.4±3.38868.4±7.0017.7±1.2148.8±1.94
      HM2H883.8±4.92792.2±6.3118.8±1.5445.4±1.02
      V893.4±7.94807.6±8.2117.4±1.5648.0±1.41
      HM3H936.6±4.84848.6±3.2619.1±1.7747.0±2.97
      V955.8±4.71865.6±2.9417.6±2.2748.4±1.02
      GB/T 25137-201089582810.025.0
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    Zhen Dou, Yuyue Wang, Anfeng Zhang, Mengjie Wu, Puqiang Wang. Effect of Different Heat Treatments on Microstructure, Properties, and Anisotropy of SLM TC4[J]. Chinese Journal of Lasers, 2022, 49(8): 0802009

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    Paper Information

    Category: laser manufacturing

    Received: Jul. 13, 2021

    Accepted: Oct. 8, 2021

    Published Online: Mar. 25, 2022

    The Author Email: Anfeng Zhang (zhangaf@mail.xjtu.edu.cn)

    DOI:10.3788/CJL202149.0802009

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