Acta Photonica Sinica, Volume. 53, Issue 11, 1114001(2024)

Effect of Hot Isostatic Pressing on Properties of Yb∶YAG Composite Laser Crystals

Zhao CHEN1,2,3, Wenpeng LIU1,3、**, Yu SUN1,3, Jinhong JIANG1,2,3, Jinyun GAO1,3, Xiaofei WANG1,3, Guihua SUN1,3, Renqin DOU1,3, Deming ZHANG1,3, Jianqiao LUO1,3, and Qingli ZHANG1,3、*
Author Affiliations
  • 1Anhui Provincial Key Laboratory of Photonic Devices and Materials,Anhui Institute of Optics and Fine Mechanics,Hefei Institutes of Physical Science,Chinese Academy of Sciences,Hefei 230031,China
  • 2University of Science and Technology of China,Hefei 230026,China
  • 3Advanced Laser Technology Laboratory of Anhui Province,Hefei 230037,China
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    Figures & Tables(16)
    Thermal bonded crystal elements
    Hot isostatic pressing process
    Experimental results of hot isostatic pressure
    SEM images of bonding surface before and after hot isostatic pressing
    Three-point bending method for measuring the flexural strength
    D Vickers hardness and fracture toughness measurement by indentation method
    Element Vickers hardness test diagram
    Transmittance spectra of elements 1,2,3 and single crystal Yb∶YAG in the range of 250~3 000 nm
    Schematic of optical uniformity test
    R2 wavefront error measurement results for element 1 and 3
    Optical uniformity distribution of single crystal Yb∶YAG
    Optical uniformity distribution of element 3
    • Table 1. Hot isostatic pressure parameters

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      Table 1. Hot isostatic pressure parameters

      Element

      Temperature rate/

      (℃·min-1

      Maximum

      temperature/℃

      Constant temperature

      time/h

      Temperature rate/

      (℃·min-1

      Maximum

      pressure/MPa

      Element1101 4005-10160
      Element2101 6005-10170
      Element3101 6005-10170
      101 6005-10170
    • Table 2. Hot isostatic pressure parameters

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      Table 2. Hot isostatic pressure parameters

      Element

      Maximum flexure

      load/N

      Flexure extension at maximum flexure load/mmFlexure stress at maximum flexure load/MPa

      Elasticity modulus/

      GPa

      Element 183.214 40.181 5104.625288.365 089 4
      Element 2170.5870.169214.854298.487
      Element 3216.9720.176 5298.487308.799 814 4
      Single Yb∶YAG221.2490.190 07318.823310.781 302 7
    • Table 3. Vickers hardness value of the element

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      Table 3. Vickers hardness value of the element

      Elementd1d2Vickers-hardness
      Element 120.521.31 270.4
      Element 221.319.41 341.9
      Element 319.019.81 475.4
      Single Yb∶YAG19.818.91 489.8
    • Table 4. Optical uniformity value of the element

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      Table 4. Optical uniformity value of the element

      CrystalOptical uniformity/(×10-6Thickness/mm
      Single Yb∶YAG5.72.78
      Yb∶YAG/Yb∶YAG7.72.78
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    Zhao CHEN, Wenpeng LIU, Yu SUN, Jinhong JIANG, Jinyun GAO, Xiaofei WANG, Guihua SUN, Renqin DOU, Deming ZHANG, Jianqiao LUO, Qingli ZHANG. Effect of Hot Isostatic Pressing on Properties of Yb∶YAG Composite Laser Crystals[J]. Acta Photonica Sinica, 2024, 53(11): 1114001

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    Paper Information

    Category:

    Received: Mar. 29, 2024

    Accepted: Jun. 27, 2024

    Published Online: Jan. 8, 2025

    The Author Email: Wenpeng LIU (wpliu@aiofm.ac.cn), Qingli ZHANG (zql@aiofm.ac.cn)

    DOI:10.3788/gzxb20245311.1114001

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