Laser & Optoelectronics Progress, Volume. 58, Issue 15, 1516012(2021)

Research Status on Radiation Performance and Radiation Resistance Technology of Rare-Earth-Doped Fibers

Bo Wang, Chi Cao, Yingbin Xing, Gui Chen, Nengli Dai, Haiqing Li, Jinggang Peng, and Jinyan Li*
Author Affiliations
  • Wuhan National Laboratory for Optoelectronics, Huazhong University of Science and Technology, Wuhan, Hubei 430074, China
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    Figures & Tables(29)
    EYDFA architecture and scheme of the irradiation test setup[61]
    Normalized gain degradation as a function of the total accumulated dose for the three fibers[61]
    Influence of the doping with Er3+ ions on the fiber radiation sensitivity[67]
    Measured RIA spectra of fibers exposed to 3.0 kGy of irradiation for 8 months[72]
    RIA and Gaussian-fitted results for the fibers exposed to 100 krad of 60Co gamma-ray irradiation[74]
    Fabrication process steps for nanoparticules erbium-doped fibers[75]
    Optical power decrease for each EDFA configuration after radiation[75]
    Schematic representation of the irradiated fiber being bleached by D2
    Irradiation dose dependence of the normalized gain of the four amplifiers[77]
    HACC fiber structure and experimental setup used for the characterization of the radiation response of EDFA[81]. (a) Fiber structure; (b) experimental setup
    Radiation induced degradation in the gain of the EDFAs designed with HACC and RTAC[81]
    Experimental setup used to measure the laser property of TDF[82]
    Laser output power of 2 μm pristine TDF, the TDFs with H2-loading and D2-loading, the irradiated TDFs, and the irradiated TDFs with H2-loading and D2-loading versus the launched pump power[82]
    Flow chart of sample preparation and test[83]
    RIA-spectra at the maximum dose 1 MGy of the four tested fibers (the inset shows the differences of RIA)[85]
    Spectral decomposition of the difference of RIA between the F2D3-O2 and F2D3 at 1 MGy[85]
    RIA spectra of GeD2 and GeD2O2 irradiated at 1 MGy (the inset shows the RIA at 350 nm)[86]
    Absorption spectra and output characteristics of laser oscillator[94]. (a) Absorption spectra of a new fiber (upper graph) and a photobleached (lower graph) fiber; (b) output characteristics of the laser oscillator using the new fiber (circles) and photobleached (squares) fiber
    Output power of three kinds of TDFs versus launched pump power[98]
    PD induced excess loss at 633, 702, 810, and 1041 nm for the pristine fiber and the 532 nm pre-irradiated fiber[99]. (a) Pristine fiber; (b) 532 nm pre-irradiated fiber
    Effect of 532 nm laser injection on optical fiber properties[99]. (a) Absorption spectra change for 532 nm and 915 nm injection; (b) PD and photo-bleaching evolution under different pump powers of 532 nm laser at 702 nm
    • Table 1. Common point defects in pure silica fibers and single-doped fibers

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      Table 1. Common point defects in pure silica fibers and single-doped fibers

      TypeFull nameAbbreviationOA peak(FWHM) /eV
      Pure-silica related point defectsOxygen deficient centerODC(Ⅰ)7.6(0.5)20-21
      ODC(Ⅱ)5.05(0.32)20-21
      3.15(0.3)20,6.9(0.4)20
      Non-bridging oxygen hole centerNBOHC2.0(0.18)20,4.8(1.0)2022
      6.8(1.8)23
      Peroxy linkagePOL3.8(0.2),4.2(0.6),7.3(0.2),7.5(0.1)24
      Peroxy radicalPOR2.08, 2.19, 5.525
      Self-trapped electronSTE3.7(1.2)26
      Self-trapped holeSTH12.61(1.2)27,1.88(0.5)27
      STH22.16(0.9)27,1.63(0.6)27
      E’centerE’5.8(0.7)20
      Germanium-related point defectsGermanium lone pair centerGLPC5.14(0.4)28,3.829
      NoGe(1)4.41(1.39)2730
      NoGe(2)5.8(0.74-0.9)29
      Germanium E’centerGeE’6.2(1.1)30
      Germanium-related NBOHCGe-NBOHC1.97(0.26)30,3.6831
      NoGeX2.61(0.97)273032
      NoGeY1.38(0.71)27
      Phosphorus-related point defectsMeta-stable POHCm-POHC2.2(0.35),2.5(0.63)2730
      Stable POHCS-POHC3.1(0.73)2730,5.3(0.74)30
      NoP10.79(0.29)27
      NoP24.5(1.27)30
      NoP44.8(0.41)30
      Aluminum-related point defectsNoAl-OHC2.3(0.9)27,3.2(1)27,4.9(1.08)33
      Aluminum E’centerAlE’4.1(1.02)33
      NoAlX1.67-1.8234
      ImpurityHydroxyl―OH0.90,0.992.1.3114
      Chlorine related defectsCl03.26,3.6527
      Cl23.78(0.7)27
      Interstitial oxygenO20.975(0.011),1.62(0.012)20
      O34.8(0.84)2022
    • Table 2. Characteristics of tested Re-doped fibers[61]

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      Table 2. Characteristics of tested Re-doped fibers[61]

      Parameter#ErYb#ErYbCe#ErYbCe+
      Core diameter (μm)121211,5
      1st Clad diameter (μm)125125125
      2nd Clad diameter (μm)170170170
      P (wt. %)999
      Er (×1025 Ions/m32.43,32,9
      Yb (×1025 Ions/m3374339
      Ce (Ions/m3nonelevel 1level 2
      SM α @ 1.536 μm dB/m635855
      MM α @ 0.915 μm dB/m2.93.32.8
    • Table 3. Parameters of experimental optical fiber[72]

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      Table 3. Parameters of experimental optical fiber[72]

      Fiber No.Fiber designationDopant concentration (mol.%)
      Er2O3Al2O3P2O5AlPO4GeO2
      1p--12--
      2PAl--413.6-
      3AlP-2.3-17-
      4Al-4---
      5Al-Ge-4--0.05
      6AlP-Ge-1-212
      7Er-Al-Ge0.07412--0.8
      8Er-PAl0.038-4.319.4-
      9Er-Al0.0466.5---
    • Table 4. Dopant concentrations in the studied glass preforms[74]

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      Table 4. Dopant concentrations in the studied glass preforms[74]

      ErYbPGe
      Sample 10.11 wt%0.95 wt%10 wt%-MMF
      Sample 20.09 wt%0.79 wt%7.7 wt%0.79 wt%
      Sample 30.10 wt%1.2 wt%8.5 wt%1.7 wt%
      Sample 40.10 wt%0.51 wt%4.5 wt%3.2 wt%
      Sample 50.12 wt%0.69 wt%10 wt%4.0 wt%MMF
      Sample 60.09 wt%0.52 wt%8.3 wt%4.4 wt%
      Sample 70.17 wt%0.84 wt%7.3 wt%6.7 wt%SMF
    • Table 5. EDFs prepared with two processes and associated EDFA parameters[75]

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      Table 5. EDFs prepared with two processes and associated EDFA parameters[75]

      Fiber NameAl-NBAl-LBNP-AlNP-SiNP-Si+
      Erbium absorption (dB/m@1530 nm)4.712.32323.2
      Aluminum (wt%)<16-84-600
      Pump power (dBm)2323212321
      Optimal Length (m)2562.54522
      Output signal (dBm)1718161715
    • Table 6. Doping of each element in tested rare-earth optical fibers[77]

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      Table 6. Doping of each element in tested rare-earth optical fibers[77]

      FibersEr3+(wi. %)Yb3+(wt. %)Ce3+(wl. %)P(wt. %)H2pre-loading
      #10.071.50--12-
      #1H0.071.50--12Yes
      #20.071.400.6-12-
      #2H0.071.400.6-12Yes
      #3--0.6-12
      #3H--0.6-12Yes
    • Table 7. Composition of tested optical fibers in Ref.[85]

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      Table 7. Composition of tested optical fibers in Ref.[85]

      SamplesSiD3SiD3-O2F2D3F2D3-O2
      F core (w%)<0.06<0.060.15÷0.250.15÷0.25
      F clad (w%)1.5÷1.61.5÷1.61.3÷1.41.3÷1.4
      Cl core (w%)<0.1<0.1<0.1<0.1
      Cl clad (w%)<0.1<0.1<0.1<0.1
      [O2] (cm-3none~2·1018none~2·1018
    • Table 8. Mechanism, advantages and disadvantages of various anti-irradiation methods

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      Table 8. Mechanism, advantages and disadvantages of various anti-irradiation methods

      MethodMechanismAdvantageDisadvantage
      Ce co-dopingValence change of CeReduce both RIA and PDIncrease thermal effect and reduce laser efficiency
      Adjust doping ratioSee 4.1.2Simplicity of operatorDifficult to accurate proportion adjustment
      Nanoparticules doping-processReduce Al co-doping and quenching level of ErReduce the Al related color centerReduced fiber gain

      Gas loading

      (H2,D2,O2

      Reduce the corresponding point defects

      Simplicity of operator,

      radiation-hardening effect is good

      H2, D2 outdiffuse with time easily,

      O2 loading can produce peroxy defects and interstitial oxygen

      Photobleaching /heat bleachingColor centers absorb energy/heat to bleach(still in research)

      Reduce both RIA and PD,

      easy to operate

      Photobleaching requires the system to work,

      the heat bleaching temperature is too high

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    Bo Wang, Chi Cao, Yingbin Xing, Gui Chen, Nengli Dai, Haiqing Li, Jinggang Peng, Jinyan Li. Research Status on Radiation Performance and Radiation Resistance Technology of Rare-Earth-Doped Fibers[J]. Laser & Optoelectronics Progress, 2021, 58(15): 1516012

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    Paper Information

    Category: Materials

    Received: Jan. 18, 2021

    Accepted: Mar. 2, 2021

    Published Online: Aug. 6, 2021

    The Author Email: Jinyan Li (ljy@hust.edu.cn)

    DOI:10.3788/LOP202158.1516012

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