Acta Optica Sinica, Volume. 41, Issue 4, 0406002(2021)

A New Fabrication Method of Fiber Bragg Grating Hydrogen Sensor

Xin Xin1,2, Yongwu Wu1,2, Huimin Liu1,2, Junlian Chen1,2, Fei Peng1,2, and Nianbing Zhong1,2,3、*
Author Affiliations
  • 1Chongqing Key Laboratory of Optical Fiber Sensor and Photoelectric Detection, Chongqing University of Technology, Chongqing 400054, China
  • 2Chongqing Key Laboratory of Modern Photoelectric Detection Technology and Instrument, Chongqing University of Technology, Chongqing 400054, China
  • 3Liangjiang International College, Chongqing University of Technology, Chongqing 401135, China
  • show less
    Figures & Tables(15)
    Schematic diagram and process of FBG hydrogen sensor preparation
    Reflection spectra of HT-FBG and T-FBG
    Hydrogen detection system
    Fiber surface morphology characterization at various stages of polydopamine-assisted electroless palladium plating process. (a)(e) For the bare fiber; (b)(f) for PDA-loaded fiber; (c)(g) for palladium-seeds fiber; (d)(h) for electroless palladium-plated fiber with sodium hypophosphite
    Response of SELP-60 s FBG hydrogen sensor with different thickness of polydopamine coating to hydrogen concentration from 0 to 4%
    Micrographs of the PDA coating surface at different deposition time on the fiber surface. (a) 0 min; (b) 10 min; (c) 20 min; (d) 30 min
    Response to 5% H2 3 cycles and surface morphology of FBG hydrogen sensor electrolessly plated with sodium hypophosphite and hydrazine hydrate. (a)(c)(d) With sodium hypophosphite; (b)(e)(f) with hydrazine hydrate
    Cross section morphology and thickness of the palladium film under different deposition time of hydrazine hydrate electroless palladium plating. (a) Cross section of the polydopamine coating without electroless palladium plating; (b)-(f) palladium membrane sections at deposition time of 60 s, 90 s, 120 s, 150 s, and 180 s
    Effect of HELP deposition time on palladium film thickness and sensor performance. (a) Relationship between HELP deposition time and palladium film thickness; (b) response of FBG hydrogen sensor to 5% hydrogen concentration under different deposition time; (c) variation trend of sensor sensitivity and response time with palladium film thickness
    HELP-120 s FBG hydrogen sensor response to hydrogen cycle and response of hydrogen with different concentrations. (a) Sensor response with time; (b) sensor response with hydrogen concentration
    Surface topography of FBG hydrogen sensor before and after coating with hydrophobic film. (a) Before coating; (b) after coating
    Effect of hydrophobic film coating layer number and relative humidity on sensor performance. (a) FBG hydrogen sensor with different hydrophobic film coating layers responds to 5% concentration hydrogen at 20%RH and 70%RH; (b) FBG hydrogen sensor coated with 15 layers of hydrophobic film responds to 5% hydrogen concentration under 20%RH-90%RH
    Temperature sensitive characteristics of HT-FBG and T-FBG and response of sensor before and after temperature compensation. (a) HT-FBG and T-FBG temperature calibration curves; (b) response of the FBG hydrogen sensor to 5% concentration H2 before and after temperature compensation at 30-70 ℃
    • Table 1. Compositions and experimental conditions of electroless palladium plating solution for sodium hypophosphite and hydrazine hydrate

      View table

      Table 1. Compositions and experimental conditions of electroless palladium plating solution for sodium hypophosphite and hydrazine hydrate

      CategorySELPHELP
      Palladium precursorPdCl2(2 g·L-1)PdCl2(2 g·L-1)
      Complexing agentEDTA(37 g·L-1)Na2EDTA(37 g·L-1)
      NH4OH(165 mL·L-1)NH4OH(265 mL·L-1)
      Stabilizing agentNH4Cl(33 g·L-1)
      Reducing agentNaPO2H2·H2O(13.2 g·L-1)N2H4·H2O(0.08 mol·L-1)
      Temperature45 ℃45 ℃
    • Table 2. Relationship of polydopamine (PDA) film thickness on silicon substrates with polymerization time (refractive index of the PDA is 1.736 at 523 nm)

      View table

      Table 2. Relationship of polydopamine (PDA) film thickness on silicon substrates with polymerization time (refractive index of the PDA is 1.736 at 523 nm)

      Polymerization time /minPDA film thickness /nm
      108.9
      2018.1
      3027.3
    Tools

    Get Citation

    Copy Citation Text

    Xin Xin, Yongwu Wu, Huimin Liu, Junlian Chen, Fei Peng, Nianbing Zhong. A New Fabrication Method of Fiber Bragg Grating Hydrogen Sensor[J]. Acta Optica Sinica, 2021, 41(4): 0406002

    Download Citation

    EndNote(RIS)BibTexPlain Text
    Save article for my favorites
    Paper Information

    Category: Fiber Optics and Optical Communications

    Received: Aug. 26, 2020

    Accepted: Oct. 9, 2020

    Published Online: Feb. 25, 2021

    The Author Email: Nianbing Zhong (zhongnianbing@163.com)

    DOI:10.3788/AOS202141.0406002

    Topics