Acta Optica Sinica, Volume. 41, Issue 4, 0406002(2021)
A New Fabrication Method of Fiber Bragg Grating Hydrogen Sensor
Fig. 4. Fiber surface morphology characterization at various stages of polydopamine-assisted electroless palladium plating process. (a)(e) For the bare fiber; (b)(f) for PDA-loaded fiber; (c)(g) for palladium-seeds fiber; (d)(h) for electroless palladium-plated fiber with sodium hypophosphite
Fig. 5. Response of SELP-60 s FBG hydrogen sensor with different thickness of polydopamine coating to hydrogen concentration from 0 to 4%
Fig. 6. Micrographs of the PDA coating surface at different deposition time on the fiber surface. (a) 0 min; (b) 10 min; (c) 20 min; (d) 30 min
Fig. 7. Response to 5% H2 3 cycles and surface morphology of FBG hydrogen sensor electrolessly plated with sodium hypophosphite and hydrazine hydrate. (a)(c)(d) With sodium hypophosphite; (b)(e)(f) with hydrazine hydrate
Fig. 8. Cross section morphology and thickness of the palladium film under different deposition time of hydrazine hydrate electroless palladium plating. (a) Cross section of the polydopamine coating without electroless palladium plating; (b)-(f) palladium membrane sections at deposition time of 60 s, 90 s, 120 s, 150 s, and 180 s
Fig. 9. Effect of HELP deposition time on palladium film thickness and sensor performance. (a) Relationship between HELP deposition time and palladium film thickness; (b) response of FBG hydrogen sensor to 5% hydrogen concentration under different deposition time; (c) variation trend of sensor sensitivity and response time with palladium film thickness
Fig. 10. HELP-120 s FBG hydrogen sensor response to hydrogen cycle and response of hydrogen with different concentrations. (a) Sensor response with time; (b) sensor response with hydrogen concentration
Fig. 11. Surface topography of FBG hydrogen sensor before and after coating with hydrophobic film. (a) Before coating; (b) after coating
Fig. 12. Effect of hydrophobic film coating layer number and relative humidity on sensor performance. (a) FBG hydrogen sensor with different hydrophobic film coating layers responds to 5% concentration hydrogen at 20%RH and 70%RH; (b) FBG hydrogen sensor coated with 15 layers of hydrophobic film responds to 5% hydrogen concentration under 20%RH-90%RH
Fig. 13. Temperature sensitive characteristics of HT-FBG and T-FBG and response of sensor before and after temperature compensation. (a) HT-FBG and T-FBG temperature calibration curves; (b) response of the FBG hydrogen sensor to 5% concentration H2 before and after temperature compensation at 30-70 ℃
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Xin Xin, Yongwu Wu, Huimin Liu, Junlian Chen, Fei Peng, Nianbing Zhong. A New Fabrication Method of Fiber Bragg Grating Hydrogen Sensor[J]. Acta Optica Sinica, 2021, 41(4): 0406002
Category: Fiber Optics and Optical Communications
Received: Aug. 26, 2020
Accepted: Oct. 9, 2020
Published Online: Feb. 25, 2021
The Author Email: Nianbing Zhong (zhongnianbing@163.com)