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Acta Optica Sinica, Volume. 40, Issue 18, 1831001(2020)

In-Situ Electrochemical-Photoreduction Synthesis and Photocatalytic Performance of Pd/BiF3 Thin Films

Ruigang Hao1、*, Xiangpeng Kong2, Zu Zhao3, and Xiaochao Zhang3、**
Author Affiliations
  • 1Department of Environmental and Safety Engineering, Taiyuan Institute of Technology, Taiyuan, Shanxi 0 30008, China
  • 2Department of Chemistry and Chemical Engineering, Taiyuan Institute of Technology, Taiyuan, Shanxi 0 30008, China
  • 3College of Chemistry and Chemical Engineering, Taiyuan University of Technology, Taiyuan, Shanxi 0 30024, China
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    XRD patterns of BiF3 and Pd/BiF3 thin films

    Fig. 1. XRD patterns of BiF3 and Pd/BiF3 thin films

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    Photocatalytic activities of BiF3 thin films before and after loading Pd. (a) Photocatalytic degradation of RhB; (b) kinetic rate constants; (c) photocatalytic recycling experiments of Pd(2.0%)/BiF3 thin film

    Fig. 2. Photocatalytic activities of BiF3 thin films before and after loading Pd. (a) Photocatalytic degradation of RhB; (b) kinetic rate constants; (c) photocatalytic recycling experiments of Pd(2.0%)/BiF3 thin film

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    XPS spectra of Pd(2.0%)/BiF3 thin film. (a) Survey; (b) Bi 4f; (c) F ls; (d) Pd 4f

    Fig. 3. XPS spectra of Pd(2.0%)/BiF3 thin film. (a) Survey; (b) Bi 4f; (c) F ls; (d) Pd 4f

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    SEM images and EDS analysis of Pd/BiF3 thin film. (a) BiF3;(b) Pd(1.0%)/BiF3; (c) Pd(2.0%)/BiF3; (d) Pd(4.0%)/BiF3;(e)EDS analysis of Pd(2.0%)/BiF3 thin film

    Fig. 4. SEM images and EDS analysis of Pd/BiF3 thin film. (a) BiF3;(b) Pd(1.0%)/BiF3; (c) Pd(2.0%)/BiF3; (d) Pd(4.0%)/BiF3;(e)EDS analysis of Pd(2.0%)/BiF3 thin film

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    Optical and electrical performances of BiF3 and Pd(2.0%)/BiF3 thin films. (a) Transient photocurrent curves; (b) UV-Vis DRS patterns

    Fig. 5. Optical and electrical performances of BiF3 and Pd(2.0%)/BiF3 thin films. (a) Transient photocurrent curves; (b) UV-Vis DRS patterns

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    Photocatalytic mechanism of Pd(2.0%)/BiF3 thin film. (a) Capture experiment of active species; (b) photocatalytic reaction mechanism

    Fig. 6. Photocatalytic mechanism of Pd(2.0%)/BiF3 thin film. (a) Capture experiment of active species; (b) photocatalytic reaction mechanism

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    Ruigang Hao, Xiangpeng Kong, Zu Zhao, Xiaochao Zhang. In-Situ Electrochemical-Photoreduction Synthesis and Photocatalytic Performance of Pd/BiF3 Thin Films[J]. Acta Optica Sinica, 2020, 40(18): 1831001

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    Paper Information

    Category: Thin Films

    Received: Mar. 25, 2020

    Accepted: Jun. 3, 2020

    Published Online: Aug. 28, 2020

    The Author Email: Hao Ruigang (tyhaorg@163.com), Zhang Xiaochao (zhangxiaochao@tyut.edu.cn)

    DOI:10.3788/AOS202040.1831001

    Topics

    laser devices and laser physics
    Lasers and Laser Optics
    Laser physics
    laser manufacturing
    Instrumentation, Measurement and Metrology