Chinese Journal of Lasers, Volume. 51, Issue 20, 2002305(2024)

Research on Defect Control and Crystal Directional Growth of DD6 Single Crystal Superalloy Prepared Using Laser Directed Energy Deposition

Zhixu Xu1, Yanhua Zhao1、*, Weifang Xie1, Xiuping Han1, Yanle Li2, Hua Tian3, Lei Chen4, and Bin Tan3
Author Affiliations
  • 1School of Mechanical and Electronic Engineering, Shandong Jianzhu University, Jinan 250101, Shandong , China
  • 2School of Mechanical Engineering, Shandong University, Jinan 250061, Shandong , China
  • 3Logistics Management Office, Shandong Jianzhu University, Jinan 250101, Shandong , China
  • 4School of Production-Education Integration, Shandong Jianzhu University, Jinan 250101, Shandong , China
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    Figures & Tables(18)
    Experimental materials and method. (a) Morphology of DD6 alloy powder; (b) substrate; (c) deposited sample; (d) sample area division and quantitative size
    Cross-sectional microstructures in single-channel single-layer laser deposition under different laser powers. (a) 400 W; (b) 600 W; (c) 800 W; (d)1000 W; (e) 1200 W; (f) 1400 W
    Cross-sectional microstructures of samples when laser power is 800 W. (a) Scanning speed is 5 mm/s and powder feeding rate is 5 g/min; (b) scanning speed is 10 mm/s and powder feeding rate is 10 g/min; (c) scanning speed is 15 mm/s and powder feeding rate is 15 g/min; (d)(e)(f) local microstructures
    Cross-sectional microstructures of samples when laser power is 1000 W. (a) Scanning speed is 5 mm/s and powder feeding rate is 15 g/min; (b) scanning speed is 10 mm/s and powder feeding rate is 5 g/min; (c) scanning speed is 15 mm/s and powder feeding rate is 10 g/min; (d)(e)(f) local microstructures
    Cross-sectional microstructures of samples when laser power is 1200 W. (a) Scanning speed is 5 mm/s and powder feeding rate is 10 g/min; (b) scanning speed is 10 mm/s and powder feeding rate is 15 g/min; (c) scanning speed is 15 mm/s and powder feeding rate is 15 g/min; (d)(e)(f) local microstructures
    Microstructures of single-channel 30-layer sample when laser power is 1000 W, scanning speed is 15 mm/s, and powder feeding rate is 10 g/min under continuous deposition strategy. (a) Overall cross-section microstructure; (b) top microstructure; (c) center microstructure; (d) bottom microstructure
    Microstructures of 4-channel 10-layer sample when laser power is 1000 W, scanning speed is 15 mm/s, and powder feeding rate is 10 g/min under continuous deposition strategy. (a) Overall cross-section microstructure; (b) top microstructure; (c) center microstructure; (d) deflection columnar crystal; (e) bottom microstructure
    Element distributions of multi-channel multi-layer sample when laser power is 1000 W, scanning speed is 15 mm/s, and powder feeding rate is 10 g/min under continuous deposition strategy. (a) Top element spectrum obtained by surface scanning; (b) bottom element spectrum obtained by surface scanning; (c) distribution of each element at top; (d) distribution of each element at bottom
    Microstructure and crystal orientation distributions of single-channel multi-layer sample when laser power is 1000 W, scanning speed is 15 mm/s, and powder feeding rate is 10 g/min under intermittent deposition strategy. (a) Microstructure of sedimentary area; (b) top crystal orientation distribution; (c) bottom crystal orientation distribution; (d) bottom pole diagram
    Microstructure and crystal orientation distributions of multi-channel multi-layer sample when laser power is 1000 W, scanning speed is 15 mm/s, and powder feeding rate is 10 g/min under intermittent deposition strategy. (a) Microstructure of sedimentary area; (b) top microstructure; (c) center microstructure; (d) bottom microstructure; (e) top crystal orientation distribution; (f) bottom crystal orientation distribution; (g) bottom pole diagram
    Distributions and statistical results of crystal orientation differences at bottom of deposition areas of single-channel multi-layer and multi-channel multi-layer samples under intermittent deposition strategy. (a) Distribution of crystal orientation difference at bottom of deposition area of single-channel multi-layer sample; (b) distribution of crystal orientation difference at bottom of deposition area of multi-channel multi-layer sample; (c) statistical result of crystal orientation difference at bottom of deposition area of single-channel multi-layer sample; (d) statistical result of crystal orientation difference at bottom of deposition area of multi-channel multi-layer sample
    • Table 1. Chemical compositions of DD6 Nickel-based single crystal high temperature alloy powder

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      Table 1. Chemical compositions of DD6 Nickel-based single crystal high temperature alloy powder

      ElementCrCoMoWTaReNbTiAlHfNi
      Mass fraction /%4.6609.0902.0007.4406.6701.8200.8600.0755.8600.150Bal.
    • Table 2. Single-channel single-layer L9(34) orthogonal experimental parameters

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      Table 2. Single-channel single-layer L9(34) orthogonal experimental parameters

      SampleNo.Laserpower /WScanningspeed /(mm/s)Powder feedingrate /(g/min)
      A180055
      A28001010
      A38001515
      B11000515
      B21000105
      B310001510
      C11200510
      C212001015
      C31200155
    • Table 3. Factor levels

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      Table 3. Factor levels

      LevelLaser power /WScanningspeed /(mm/s)Powder feeding rate /(g/min)
      180055
      210001010
      312001515
    • Table 4. Single-channel single-layer L9(34) orthogonal experimental data

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      Table 4. Single-channel single-layer L9(34) orthogonal experimental data

      Sample

      No.

      Level

      Directional growth height

      of crystals HE /µm

      Molten pool depth HR /µmDeposition height HD /µmCrystal directional growthratio HE/HR+HD) /%
      PVbm
      A1111338.92687.5448.1646.06
      A2122564.49477.22219.7380.99
      A3133494.68400.95121.3294.72
      B1213498.64522.49438.5451.89
      B2221350.23594.6188.5051.27
      B3232474.55392.50257.3073.02
      C1312442.75642.41348.2344.69
      C2323536.43486.72376.0862.17
      C3331494.13470.05163.1678.04
    • Table 5. Range analysis of HE/(HR+HD

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      Table 5. Range analysis of HE/(HR+HD

      FactorK1 /%K2 /%K3 /%Kavg1 /%Kavg2 /%Kavg3 /%R /%
      Laser power176.18184.90221.7758.7361.6373.9215.2
      Scanning speed194.43245.78142.6464.8181.9347.5534.38
      Powder feeding rate198.70208.78175.3766.2369.5958.4611.14
    • Table 6. Range analysis of HE

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      Table 6. Range analysis of HE

      FactorK1 /μmK2 /μmK3 /μmKavg1 /μmKavg2 /μmKavg3 /μmR /μm
      Laser power1323.421473.321398.09441.14491.11466.0349.97
      Scanning speed1451.151463.361280.31483.72487.79426.7761.02
      Powder feeding rate1481.781529.761183.28493.93509.92394.43115.49
    • Table 7. Range analysis of HD

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      Table 7. Range analysis of HD

      FactorK1 /μmK2 /μmK3 /μmKavg1 /μmKavg2 /μmKavg3 /μmR /μm
      Laser power784.34887.46389.21261.45295.82129.74166.08
      Scanning speed684.31541.78834.93228.10180.59278.3197.72
      Powder feeding rate825.26935.94299.81275.09311.9899.94212.04
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    Zhixu Xu, Yanhua Zhao, Weifang Xie, Xiuping Han, Yanle Li, Hua Tian, Lei Chen, Bin Tan. Research on Defect Control and Crystal Directional Growth of DD6 Single Crystal Superalloy Prepared Using Laser Directed Energy Deposition[J]. Chinese Journal of Lasers, 2024, 51(20): 2002305

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    Paper Information

    Category: Laser Additive Manufacturing

    Received: Jan. 15, 2024

    Accepted: Apr. 2, 2024

    Published Online: Oct. 12, 2024

    The Author Email: Zhao Yanhua (zyh@sdjzu.edu.cn)

    DOI:10.3788/CJL240501

    CSTR:32183.14.CJL240501

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