Chinese Journal of Lasers, Volume. 51, Issue 10, 1002309(2024)

Microstructure Toughening and Properties of Selective Laser Melted NbMoTaW Refractory High‑Entropy Alloys (Invited)

Jintao Xu1, Qingjun Zhou2, Zhenyu Yan2, Donglai Li2, Shangzhe Du1, Ran Duan1, Junhao Sun3, Kai Feng1、*, and Zhuguo Li1
Author Affiliations
  • 1School of Materials Science and Engineering, Shanghai Jiao Tong University, Shanghai 200240, China
  • 2Capital Aerospace Machinery Co., Ltd., Beijing 100076, China
  • 3SJTU-Yibin Innovation Center for Advanced Materials, Yibin 644000, Sichuan , China
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    Figures & Tables(14)
    Characterization of NbMoTaW alloy powder. (a) NbMoTaW powder morphology; (b) particle size distribution
    Schematics of test process. (a) Diagram of SLM process; (b) diagram of scanning strategy
    Forming and densification analysis results of (NbMoTaW)100-xCx sample. (a) Forming quality observed by optical microscope(OM); (b) forming quality observed by SEM; (c) 3D-CT result and pore volume distribution
    XRD pattern of (NbMoTaW)100-xCx RHEAs
    EBSD analysis and energy dispersive spectrometer (EDS) characterization results of (NbMoTaW)100-xCx RHEA[24]. (a) Inverse pole figure (IPF) of (NbMoTaW)99.5C0.5; (b) IPF of NbMoTaW; (c) KAM and EDS images of (NbMoTaW)99.5C0.5 RHEA; (d) KAM and EDS images of NbMoTaW
    EBSD statistics results of (NbMoTaW)100-xCxRHEA. (a) Grain size distribution; (b) grain boundary misorientation distribution;(c) kernel misorientation distribution
    TEM characterization analysis results of (NbMoTaW)100-xCx samples[24]. (a) TEM micrograph, TEM dark-field image, and corresponding SAED spots of NbMoTaW; (b) TEM micrograph, TEM dark-field image, and corresponding SAED spots of (NbMoTaW)100-xCx RHEA; (c) STEM morphology and EDS analysis result; (d) TEM image of (NbMoTaW)99.5C0.5 RHEA at grain boundary; (e) HRTEM image of (NbMoTaW)99.5C0.5 around dislocations; (f) HRTEM image of (NbMoTaW)99.5C0.5 at grain boundary
    Analysis and characterization of mechanical properties of (NbMoTaW)100-xCx sample. (a) Compressive stress-strain curves of (NbMoTaW)100-xCx RHEAs; (b) fracture morphology of NbMoTaW; (c) fracture morphology of (NbMoTaW)99.5C0.5
    XRD patterns of NbMoTaWTix RHEAs
    Microstructures of NbMoTaWTix RHEAs. (a) NbMoTaWTi0.125; (b) NbMoTaWTi0.250; (c) NbMoTaWTi0.500
    EBSD (left) and EDS (right) analysis results of NbMoTaWTix RHEAs. (a) NbMoTaWTi0.125; (b) NbMoTaWTi0.250;
    Analysis and characterization of mechanical properties of NbMoTaWTix samples. (a) Compressive stress-strain curves of NbMoTaWTix RHEAs; (b) yield strength and compressive strain versus Ti atomic fraction
    • Table 1. Chemical compositions of NbMoTaWTix RHEAs (atomic fraction, %)

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      Table 1. Chemical compositions of NbMoTaWTix RHEAs (atomic fraction, %)

      AlloyNbMoTaWTi
      NbMoTaW25.0025.0025.0025.000
      NbMoTaWTi0.12524.2424.2424.2424.243.03
      NbMoTaWTi0.25023.5323.5323.5323.535.88
      NbMoTaWTi0.50022.2222.2222.2222.2211.11
    • Table 2. Compression properties of NbMoTaWTix RHEAs

      View table

      Table 2. Compression properties of NbMoTaWTix RHEAs

      Metalσ0.2 /MPaσp /MPaεp /%
      NbMoTaW1183±151214±193.9±0.2
      NbMoTaWTi0.1251381±201461±255.3±0.6
      NbMoTaWTi0.2501422±131580±77.2±0.5
      NbMoTaWTi0.5001428±241587±88.5±0.7
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    Jintao Xu, Qingjun Zhou, Zhenyu Yan, Donglai Li, Shangzhe Du, Ran Duan, Junhao Sun, Kai Feng, Zhuguo Li. Microstructure Toughening and Properties of Selective Laser Melted NbMoTaW Refractory High‑Entropy Alloys (Invited)[J]. Chinese Journal of Lasers, 2024, 51(10): 1002309

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    Paper Information

    Category: Laser Additive Manufacturing

    Received: Dec. 26, 2023

    Accepted: Mar. 25, 2024

    Published Online: Apr. 26, 2024

    The Author Email: Feng Kai (fengkai@sjtu.edu.cn)

    DOI:10.3788/CJL231581

    CSTR:32183.14.CJL231581

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