Chinese Journal of Lasers, Volume. 51, Issue 10, 1002309(2024)
Microstructure Toughening and Properties of Selective Laser Melted NbMoTaW Refractory High‑Entropy Alloys (Invited)
Fig. 1. Characterization of NbMoTaW alloy powder. (a) NbMoTaW powder morphology; (b) particle size distribution
Fig. 2. Schematics of test process. (a) Diagram of SLM process; (b) diagram of scanning strategy
Fig. 3. Forming and densification analysis results of (NbMoTaW)100-xCx sample. (a) Forming quality observed by optical microscope(OM); (b) forming quality observed by SEM; (c) 3D-CT result and pore volume distribution
Fig. 5. EBSD analysis and energy dispersive spectrometer (EDS) characterization results of (NbMoTaW)100-xCx RHEA[24]. (a) Inverse pole figure (IPF) of (NbMoTaW)99.5C0.5; (b) IPF of NbMoTaW; (c) KAM and EDS images of (NbMoTaW)99.5C0.5 RHEA; (d) KAM and EDS images of NbMoTaW
Fig. 6. EBSD statistics results of (NbMoTaW)100-xCxRHEA. (a) Grain size distribution; (b) grain boundary misorientation distribution;(c) kernel misorientation distribution
Fig. 7. TEM characterization analysis results of (NbMoTaW)100-xCx samples[24]. (a) TEM micrograph, TEM dark-field image, and corresponding SAED spots of NbMoTaW; (b) TEM micrograph, TEM dark-field image, and corresponding SAED spots of (NbMoTaW)100-xCx RHEA; (c) STEM morphology and EDS analysis result; (d) TEM image of (NbMoTaW)99.5C0.5 RHEA at grain boundary; (e) HRTEM image of (NbMoTaW)99.5C0.5 around dislocations; (f) HRTEM image of (NbMoTaW)99.5C0.5 at grain boundary
Fig. 8. Analysis and characterization of mechanical properties of (NbMoTaW)100-xCx sample. (a) Compressive stress-strain curves of (NbMoTaW)100-xCx RHEAs; (b) fracture morphology of NbMoTaW; (c) fracture morphology of (NbMoTaW)99.5C0.5
Fig. 10. Microstructures of NbMoTaWTix RHEAs. (a) NbMoTaWTi0.125; (b) NbMoTaWTi0.250; (c) NbMoTaWTi0.500
Fig. 11. EBSD (left) and EDS (right) analysis results of NbMoTaWTix RHEAs. (a) NbMoTaWTi0.125; (b) NbMoTaWTi0.250;
Fig. 12. Analysis and characterization of mechanical properties of NbMoTaWTix samples. (a) Compressive stress-strain curves of NbMoTaWTix RHEAs; (b) yield strength and compressive strain versus Ti atomic fraction
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Jintao Xu, Qingjun Zhou, Zhenyu Yan, Donglai Li, Shangzhe Du, Ran Duan, Junhao Sun, Kai Feng, Zhuguo Li. Microstructure Toughening and Properties of Selective Laser Melted NbMoTaW Refractory High‑Entropy Alloys (Invited)[J]. Chinese Journal of Lasers, 2024, 51(10): 1002309
Category: Laser Additive Manufacturing
Received: Dec. 26, 2023
Accepted: Mar. 25, 2024
Published Online: Apr. 26, 2024
The Author Email: Feng Kai (fengkai@sjtu.edu.cn)
CSTR:32183.14.CJL231581