High Power Laser and Particle Beams, Volume. 36, Issue 10, 106002(2024)

A review of multi-field coupled in-situ stretching neutron diffraction experimental devices

Haibiao Zheng1,2,3, Le Kang1,3, Jie Chen1,3, and Xuekai Zhang1,3
Author Affiliations
  • 1Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049, China
  • 2University of Chinese Academy of Sciences, Beijing 100049, China
  • 3Spallation Neutron Source Science Center, Dongguan 523803, China
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    Figures & Tables(12)
    Design principle diagram of neutron in-situ experiment in stretching device
    Principle diagram of in-situ experiment at room temperature using horizontal stretching device of Vulcan
    Principle diagram of in-situ neutron diffraction measurement for lithium batteries
    Experimental setup and sample clamping in the loading device and placed on the spectrometer platform[26]
    Schematic diagram of in-situ neutron diffraction measurement for loading with O-ring
    Schematic diagram of the principle of magnetic field coupling stretching experiment measurement
    Schematic diagram of in-situ neutron diffraction measurement using low-temperature coupled stretching device of SMARTS
    Principle diagram of in-situ neutron diffraction measurement using low-temperature coupled stretching device of SANS
    Principle diagram of in-situ neutron diffraction measurement using high-temperature coupled stretching device of Vulcan
    Diagram of magnetic field coupling in-situ stretching device and its experimental analysis
    • Table 1. Advantages and disadvantages of different heating methods

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      Table 1. Advantages and disadvantages of different heating methods

      heating methodadvantagedisadvantage
      heating elementyou can choose different models based on different temperature rangeslow heating efficiency
      thermal induction coilthe heating efficiency is over 80%, and it can be heated to extremely high temperatures with minimal impact on the surrounding temperaturethere is a temperature gradient change around it
      DC heatingDC current has a fast heating speed and can heat up to extremely high temperatures, with little impact on the surrounding temperaturepoor heating effect on samples with good conductivity
      halogen lampthe heating speed is fast and can reach extremely high temperatures, with little impact on the surrounding temperaturehalogen lamps need to be placed around the sample, which may require gas protection such as vacuum
      laserthe heating speed is fast and can reach extremely high temperatures, with little impact on the surrounding temperaturepoint light source heating with temperature gradient
    • Table 2. Comparison of partial stretching devices

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      Table 2. Comparison of partial stretching devices

      subordinate deviceneutron instrumentloading structuremaximum loadsample environmentloading method
      American Spallation Neutron Source (SNS)Vulcanhorizontal uniaxial biaxial stretching 1100 kNnormal atmospheric temperaturestretching or compressing
      horizontal uniaxial biaxial stretching 2100 kN400 N·melectrochemistrytension compression, fatigue, creep, and torsion
      Spallation Neutron Source, UK (ISIS)Engin-Xvertical uniaxial uniaxial tension50 kNnormal atmospheric temperaturetension, compression, fatigue
      Los Alamos National Laboratory, USA(LANSCE)SMARTSuniaxial biaxial stretching250 kNlow temperaturepull and press
      Japan High Current Proton Accelerator Facility (J-PARC)TAKUMIhorizontal uniaxial uniaxial tension50 kNlow temperature, high temperaturepull and press
      China Academy of Engineering Physics Mianyang Research Reactor (CMRR)RSNDhorizontal uniaxial uniaxial tension2.5 kNlow temperaturepull and press
      China Spallation Neutron Source (CSNS)CSNSvertical or horizontal50 kNhigh temperature, low temperature, magnetic fieldtension, compression, fatigue
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    Haibiao Zheng, Le Kang, Jie Chen, Xuekai Zhang. A review of multi-field coupled in-situ stretching neutron diffraction experimental devices[J]. High Power Laser and Particle Beams, 2024, 36(10): 106002

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    Paper Information

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    Received: Jun. 21, 2024

    Accepted: Sep. 6, 2024

    Published Online: Nov. 13, 2024

    The Author Email:

    DOI:10.11884/HPLPB202436.240207

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