NUCLEAR TECHNIQUES, Volume. 47, Issue 12, 120401(2024)

Design and development of fluorescence gas detector for X-ray absorption fine structure

Yu CHEN1, Jiandong WANG2, Shijie PU2, Qian GAO1, Tao GAN1, Yuying HUANG1,2, Shuo ZHANG1,2, and Jiong LI1,2、*
Author Affiliations
  • 1Shanghai Advanced Research Institute, Chinese Academy of Sciences, Shanghai 201210, China
  • 2Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800, China
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    Figures & Tables(14)
    Structural diagram of filter and slit assembly
    Simulation model built by Geant4
    Energy spectra of X-rays entering the detector obtained by simulation (a) Without the filter and the slit; (b) With the filter of 12.3 μm (~3 absorption lengths) thickness, and without slit; (c) With the filter of 12.3 μm thickness and the slit; (d) With only the filter of 24.6 μm (~6 absorption lengths) thickness; (e) With the filter of 24.6 μm thickness and the slit
    Schematic diagram of the internal structure of multi-layer grid ionization chamber
    Principle diagram of multi-layer grid ionization chamber detection (color online)
    Schematic diagram of XAFS data acquisition system of BL11B beamline
    Digitized noise box plot of fluorescence gas detector and Lytle detector (color online)
    Layout of intrinsic response time measurement of multi-grid fluorescent ionization chamber
    Rise time of multi-grid fluorescent ionization chamber under different high voltages
    Relationship between the applied voltage and the output intensity of fluorescence gas detector
    Relationship between output intensity of fluorescence gas detector and incident X-ray intensity
    Original XAFS spectrum of the same sample measured by self-developed fluorescence gas detector and Lytle detector respectively. The insets show k-weighted EXAFS in k space (a) XAFS of Cu sample with 0.1 wt% Cu, (b) XAFS of Co3O4 with 1 wt% Co, (c) XAFS of Pt/ZEO with 0.5 wt% Pt, (d) XAFS of Mo-Ru sample with 0.2 wt% Mo
    • Table 1. Test results of amplifier module

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      Table 1. Test results of amplifier module

      增益

      Gain / V·A-1

      上升时间

      Rise time / ms

      噪声水平

      Noise level / mV

      基线

      Baseline / mV

      1091.0000.427 6-2.529 8
      10108.1481.054 0-2.943 3
    • Table 2. Noise statistics of fluorescence gas detector and Lytle detector

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      Table 2. Noise statistics of fluorescence gas detector and Lytle detector

      测量序号

      Items

      标准差

      Standard deviation / V

      方差

      Variance / V

      G-15.646 83×10-53.188 67×10-9
      G-25.671 02×10-53.216 04×10-9
      G-35.702 44×10-53.251 79×10-9
      L-19.951 91×10-59.904 05×10-9
      L-29.537 02×10-59.095 48×10-9
      L-31.059 16×10-41.121 81×10-8
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    Yu CHEN, Jiandong WANG, Shijie PU, Qian GAO, Tao GAN, Yuying HUANG, Shuo ZHANG, Jiong LI. Design and development of fluorescence gas detector for X-ray absorption fine structure[J]. NUCLEAR TECHNIQUES, 2024, 47(12): 120401

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    Paper Information

    Category: NUCLEAR ELECTRONICS AND INSTRUMENTATION

    Received: Mar. 25, 2024

    Accepted: --

    Published Online: Jan. 15, 2025

    The Author Email: LI Jiong (LIJiong)

    DOI:10.11889/j.0253-3219.2024.hjs.47.120401

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