Acta Optica Sinica, Volume. 40, Issue 3, 0334001(2020)

Synchrotron Radiation Infrared Three-Dimensional Microspectroscopy Based on Point Scanning Method

Yuecheng Lin1,4, Yajun Tong2, Te Ji1,3, Weiwei Peng1,3, Tiqiao Xiao1,3, Huachun Zhu1,3、*, and Min Chen1,3、**
Author Affiliations
  • 1Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800, China
  • 2Shanghai Tech University, Shanghai 201210, China
  • 3Shanghai Synchrotron Radiation Facility, Shanghai Advanced Research Institute, Chinese Academy of Sciences, Shanghai 201204, China
  • 4University of Chinese Academy of Sciences, Beijing 100049, China
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    Figures & Tables(8)
    Experimental setup of BL01B in SSRF
    SRIR light transmission schematic and chemical structure of imide ring. (a) Schematic of SRIR light transmission; (b) chemical structure of imide loop
    IR spectrum of MiTeGen loop in wavenumber range of 1900--1000 cm-1
    MiTeGen loop. (a) Front view of visible image of MiTeGen loop; (b) SRIR microscopic spectrum of amide Ⅱ at wavenumber of 1490 cm-1
    SRIR 3D microscopic reconstruction of amide Ⅱ. (a) 0° side view; (b) 45° side view; (c) 135° side view
    Reconstruction images of amide Ⅱ at different depths. (a) Whole reconstruction image of amide Ⅱ; (b) 7.5 μm;(c) 10 μm; (d) 12.5 μm; (e) 15 μm; (f) 17.5 μm; (g) 22 μm; (h) 25 μm; (i) 27.5 μm; (j) 32.5 μm
    Arrangement of effective tomography images and intensity curve of tomography slice 8. (a) Ordered arrangement of 15 effective synchrotron radiation absorption tomography images of amide Ⅱ; (b) synchrotron radiation infrared microspectroscopy intensity profile of tomography slice 8
    • Table 1. Main components of MiTeGen loop in wavenumber range of 1900-1000 cm-1

      View table

      Table 1. Main components of MiTeGen loop in wavenumber range of 1900-1000 cm-1

      WavenumberComponentChemical bond
      1664--1538 cm-1Amide IN—H bend
      1538--1452 cm-1Amide ⅡCoupling between N—H and C—N
      1476--1372 cm-1AmideC—N stretch
      1381--1223 cm-1Amide ШCoupling between N—H and C—N
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    Yuecheng Lin, Yajun Tong, Te Ji, Weiwei Peng, Tiqiao Xiao, Huachun Zhu, Min Chen. Synchrotron Radiation Infrared Three-Dimensional Microspectroscopy Based on Point Scanning Method[J]. Acta Optica Sinica, 2020, 40(3): 0334001

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    Paper Information

    Category: X-Ray Optics

    Received: Aug. 30, 2019

    Accepted: Oct. 12, 2019

    Published Online: Feb. 10, 2020

    The Author Email: Zhu Huachun (zhuhuachun@zjlab.org.cn), Chen Min (chenmin@zjlab.org.cn)

    DOI:10.3788/AOS202040.0334001

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