Chinese Journal of Lasers, Volume. 52, Issue 11, 1103101(2025)

Preparation of Salt Spray‐Resistant WO3 Thin Films and Their Hydrogen Sensitivity Performance

Fenghong Chu, Jiameng Zhang, Anduo Hu*, Zhenglan Bian, Lu Cao, and Jiawen Han
Author Affiliations
  • College of Electronics and Information Engineering, Shanghai University of Electric Power, Shanghai 201306, China
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    Figures & Tables(19)
    Reaction mechanism of FAS and WO3 film
    Hydrophobic mechanism of WO3 film modified by FAS
    Reaction mechanism of KH-570 and WO3 film
    Preparation process of salt spray-resistant hydrogen sensitive film
    Fiber hydrogen sensing system
    Adsorption of water molecules on WO3 surface
    Film contact angles in orthogonal experiments
    Hydrogen sensitivity performance of FAS-WO3 films
    Thin film characterization. (a) SEM image of FAS-WO3 film; (b) SEM image of WO3 film; (c) EDS image of white particles; (d) FTIR images of FAS-WO3 and WO3 films
    Hydrogen sensitivity performance of KH-570 modified films with different R in salt spray environment. (a) Sensitivity;
    Dissolution of KH-570 in mixed solvent of water and ethanol
    FTIR spectra of FAS-WO3 film before and after KH-570 modification
    Contact angles of films
    Experimental environment. (a) 85% humidity environment; (b) 90% salt spray environment;
    Hydrogen sensitivity performance of films in different environments. (a) Sensitivity; (b) response time
    Repeatability response curve of modified film
    Effect of placement time on hydrogen sensitivity of film in air. (a) Sensitivity; (b) response time
    Effect of placement time on hydrogen sensitivity of film in 90% salt spray environment. (a) Sensitivity; (b) response time
    • Table 1. Design scheme of orthogonal experiment

      View table

      Table 1. Design scheme of orthogonal experiment

      Number

      FAS immersion

      concentration /(mol/L)

      FAS immersion

      time /h

      Heat treatment

      temperature /℃

      Heat treatment

      time /h

      #10.0231001
      #20.0121002
      #30.0311003
      #40.0332002
      #50.0222003
      #60.0112001
      #70.0133003
      #80.0323001
      #90.0213002
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    Fenghong Chu, Jiameng Zhang, Anduo Hu, Zhenglan Bian, Lu Cao, Jiawen Han. Preparation of Salt Spray‐Resistant WO3 Thin Films and Their Hydrogen Sensitivity Performance[J]. Chinese Journal of Lasers, 2025, 52(11): 1103101

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    Paper Information

    Category: Thin Films

    Received: Nov. 27, 2024

    Accepted: Jan. 20, 2025

    Published Online: Jun. 7, 2025

    The Author Email: Anduo Hu (huanduo2003@163.com)

    DOI:10.3788/CJL241395

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