Laser & Optoelectronics Progress, Volume. 61, Issue 21, 2114005(2024)

Parameter Modeling and Optimization of Laser Stereolithography Process for Alumina Ceramics

Zhao Zhang, Maomao Cui, Xiao Wang*, Wenkai Shen, Tao Wang, and Huixia Liu
Author Affiliations
  • School of Mechanical Engineering, Jiangsu University, Jiangsu 212013, Zhenjiang , China
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    Figures & Tables(14)
    Morphology of alumina powder, rheological properties curve of ceramic slurry and particle size distribution of Al2O3 powder with different particle sizes. (a) SEM image of Al2O3 particle; (b) rheological properties curve of ceramic slurry; (c) particle size distribution of 5 μm Al2O3 powder; (d) particle size distribution of 2 μm Al2O3 powder
    SLA ceramic forming equipment and laser scanning stereolithography process. (a) Schematic diagram of SLA ceramic forming equipment; (b) schematic diagram of laser scanning stereolithography ceramic slurry curing principle; (c) schematic diagram of stereolithography ceramic green body forming principle
    Cross-sectional morphology of bending specimens of stereolithography alumina ceramics in green, degreased and sintered bodies. (a) Cross-sectional morphology of green bodies; (b) cross-sectional morphology of sintered bodies; (c) cross-sectional morphology of degreased body; (d) localized enlargement diagram of cross-section morphology of degreased body
    Residual analysis results. (a) Comparation of actual value with predicted value of flexural strength; (b) normal distribution of standardized residuals; (c) comparation of standardized residual with predicted value
    Influence curve of each process parameter on flexural strength of bending specimens
    Response surface plot of the interaction between process parameters. (a) Interaction of scanning speed and scanning spacing (AB); (b) interaction of scanning speed and slice thickness (AC); (c) interaction of scanning speed and laser power (AD); (d) interaction of scanning spacing and slice thickness (BC); (e) interaction of scanning spacing and laser power (BD); (f) interaction of slice thickness and laser power (CD)
    Contour plot of the interaction between process parameters. (a) Interaction of scanning speed and scanning spacing (AB); (b) interaction of scanning speed and slice thickness (AC); (c) interaction of scanning speed and laser power (AD); (d) interaction of scanning spacing and slice thickness (BC); (e) interaction of scanning spacing and laser power (BD); (f) interaction of slice thickness and laser power (CD)
    Schematic diagram of overcuring of cured layer inside specimen by subsequent irradiation and changes in layer spacing between adjacent layers. (a) Overcuring induced by high exposure energy; (b) overcuring induced by low exposure energy; (c) variation of layer spacing between adjacent layers within specimen
    Cross-section of bending specimen at different stages of ceramic stereolithography process. (a) Delamination in bending specimens made at a scanning speed of 3000 mm/s; (b) delamination in bending specimens made at a hatching spacing of 0.14 mm; (c) bending specimens made at a scanning speed of 3000 mm/s produce laminar gaps at debinding stage; (d) bending specimens made at a hatching spacing of 0.14 mm produce laminar gaps at debinding stage; (e) (f) crack defects within sintered body of a bending specimens
    • Table 1. Experimental factors and levels

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      Table 1. Experimental factors and levels

      FactorVariable symbolLevel
      -101
      Scanning speed A /(mm/s)v200025003000
      Scanning spacing B /mmhs0.100.120.14
      Slice thickness C /mmTs0.100.120.14
      Laser power D /mWW150200250
    • Table 2. Box-Behnken experimental design scheme and results

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      Table 2. Box-Behnken experimental design scheme and results

      Experimental groupScanning speed /(mm/s)Scanning spacing /mmSlice thickness /mmLaser power /mWFlexural strength /MPa
      1-1-100246
      21-100202
      3-1100275
      41100227
      500-1-1236
      6001-1260
      700-11225
      80011268
      9-100-1238
      10100-1206
      11-1001259
      121001211
      130-1-10237
      1401-10252
      150-110254
      160110277
      17-10-10256
      1810-10215
      19-1010257
      201010250
      210-10-1248
      22010-1257
      230-101235
      240101270
      250000295
      260000298
      270000290
      280000285
      290000288
    • Table 3. Analysis of variance

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      Table 3. Analysis of variance

      SourceSum of squaresDegree of freedomMean square errorFPSignificant
      Proposed18863.16141347.3721.27<0.0001Significant
      A4033.3314033.3363.66<0.0001Significant
      B1541.3311541.3324.330.0002Significant
      C1752.0811752.0827.650.0001Significant
      D44.08144.080.69580.4182
      AB4140.06310.8053
      AC28912894.560.0509
      AD641641.010.3319
      BC161160.25250.6231
      BD16911692.670.1247
      CD90.25190.251.420.2525
      A²7746.6717746.67122.26<0.0001Significant
      B²1943.2111943.2130.67<0.0001Significant
      C²1751.711751.727.650.0001Significant
      Residual887.051463.36
      Lack of fit776.251077.632.80.1663Not significant
      Pure error110.8427.7
    • Table 4. Optimization criteria and weights

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      Table 4. Optimization criteria and weights

      ParameterCriteriaWeight
      GoalLow limitUpper limit
      Scanning speed /(mm/s)In range200030001
      Hatching spacing /mmIn range0.10.141
      Slice thickness /mmIn range0.10.141
      Laser power /mWIn range1502501
      Flexural strength /MPaMaximize2022981
    • Table 5. Validation of optimization results

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      Table 5. Validation of optimization results

      No.ABCDFlexural strength /MPa
      Predictive valueActual value
      123820.1280.127206299.077295
      223820.1280.127206299.077302
      323820.1280.127206299.077298
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    Zhao Zhang, Maomao Cui, Xiao Wang, Wenkai Shen, Tao Wang, Huixia Liu. Parameter Modeling and Optimization of Laser Stereolithography Process for Alumina Ceramics[J]. Laser & Optoelectronics Progress, 2024, 61(21): 2114005

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    Paper Information

    Category: Lasers and Laser Optics

    Received: Jan. 25, 2024

    Accepted: Mar. 12, 2024

    Published Online: Nov. 15, 2024

    The Author Email: Xiao Wang (wx@ujs.edu.cn)

    DOI:10.3788/LOP240599

    CSTR:32186.14.LOP240599

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