Matter and Radiation at Extremes, Volume. 9, Issue 6, 063801(2024)

A distinctive HPHT platform with different types of large-volume press subsystems at SECUF

Yufei Ge1、*, Shuailing Ma2, Cun You1, Kuo Hu1, Chuang Liu1, Yixuan Wang1, Xinglin Wang1, Xinyang Li1, Hongyu Li1, Qiang Tao1, Shuqing Jiang1, Lu Wang1, Hu Tang1, Di Yao1, Zhi He1, Xinyi Yang1, Zhaodong Liu1, Qiang Zhou1, Pinwen Zhu1, Bo Zou1, Bingbing Liu1, and Tian Cui1,2
Author Affiliations
  • 1Synergetic Extreme Condition High-Pressure Science Center, State Key Laboratory of Superhard Materials, College of Physics, Jilin University, Changchun 130012, China
  • 2Institute of High-Pressure Physics, School of Physical Scientific and Technology, Ningbo University, Ningbo 315211, China
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    Figures & Tables(11)
    Experimental research hall of the synergetic extreme condition user facility (SECUF) at Changchun.
    (a) Schematic of 20 000 t ultrahigh-pressure belt-type apparatus. (b) Main structural diagrams of this apparatus with dimensions (mm) from different aspects.
    (a) 3000 t Kawai-type high-pressure apparatus (Kawai-type LVP). (b) Kawai-type module. (c) MgSiO3–Al2O3 mineral system phase relation at different pressures and 2000 K in a previous study.19 The red circular symbol corresponds to the solubility of Al2O3 in bridgmanite in the present study, which is calibrated at 29 GPa in the phase relationship represented by the blue curve with dot symbols. Brg, bridgmanite; Cor, corundum; Gar, garnet. (d) Pressure in the chamber vs oil pressure. The curve is constructed from several sets of conventional resistance pressure calibrations and a mineral pressure calibration. En50Cor50 (En = MgSiO3, Cor = Al2O3) is the starting material for the mineral pressure calibration. The sample was obtained at a set load and a temperature of 2000 K. The solubility of Al2O3 in bridgmanite was then determined to confirm the chamber pressure using the phase relationship shown in (c). Reprinted with permission from Ge et al., Chin. J. High Pressure Phys. 38, 030201 (2024). Copyright 2024 Chinese Journal of High Pressure Physics Editorial Office.20 (e) Temperature in the high-pressure assembly vs heating power curve in an HPHT experiment at 29 GPa.
    (a) Relation of Vickers hardness/toughness to grain size of PCD-1 to PCD-6. Reprinted with permission from Lian et al., Int. J. Refract. Met. Hard Mater. 118, 106490 (2024). Copyright 2023 Elsevier Ltd. (b) Pair distribution function g(r) of bulk amorphous carbon samples AC-1 (synthesized at 20 GPa and 1000 °C) and AC-3 (synthesized at 27 GPa and 1000 °C). Gra, graphite; Dia, diamond. Reprinted with permission from Shang et al., Nature 599(7886), 599–604 (2021). Copyright 2024 Springer Nature Limited. (c) Estimated ZT values of β-Ag2S as functions of temperature at different pressures. Reprinted with permission from Zhao et al., Appl. Phys. Lett. 123, 062202 (2023). Copyright 2023 AIP Publishing LLC.26 (d) Logarithm of acoustic emission hit rates, oil pressure, and displacement as a function of time during a typical acoustic emission experiment with boron–epoxy and pyrophyllite as pressure-transmitting medium. Reprinted with permission from Ma et al., Rev. Sci. Instrum. 94, 023901 (2023). Copyright 2023 Authors, licensed under a Creative Commons Attribution (CC BY) license.
    (a) Ultrahigh temperature and static high-pressure apparatus. (b) Nested heater chamber. The heater is placed in the high-pressure vessel. (c) High-pressure vessel with connected fiber optic couplers.
    (a) High-pressure generation apparatus. (b) The piston–cylinder device is surrounded by a water cooling system (golden-colored). (c) Schematic of cell assembly to seal samples.
    Material synthesis, planetary research, and biological research in HPHT liquid environments. (a) A large-molecule pressure transmitting medium (DAPHNE 7575) is used as a structure-fortifying guest species to stabilize the prototypical MOF-5 at high pressures (>9 GPa) and enable the recovery of crystalline material upon decompression. Reprinted with permission from Baxter et al., Chem. Mater. 34(2), 768–776 (2022). Copyright 2022 American Chemical Society. (b) Temperature and pressure phase diagram of water ice. Different high-pressure ice phases corresponding to different icy satellites in the solar system.47 (c) Cartoon showing organisms known to exist in the ocean under extreme conditions.48
    NHP station. (a) 30 MN (630 bars) downstroke press with (d) D-DIA-type module. (b) 30 MN (3000 t) rotational apparatus with (e) two PE-type WC anvils. (c) 10 MN (690 bars) laboratory rapid compression press with (f) double-stage PE-type module (f).
    D-DIA press. (a) Schematic of 5/3 assembly with alumina pistons. (b) 6–6 compression mode with high-pressure shear assembly. (c) Difference compression positions of D-DIA upper and lower guide blocks. (d) Pressure calibration of conventional 5/3 assembly and shear assembly. (e) Typical signal recorded by the oscillograph during rapid compression. (f) Oil pressure jump curve obtained from this signal.
    (a) X-ray diffraction patterns of amorphous sulfur, showing rapid compression amorphization. Reprinted with permission from Shao et al., Macromolecules 40, 9475–9481 (2007). Copyright 2007 American Chemical Society.56 (b) Compression and release path in the phase diagram of Bi under HPHT. Reprinted with permission from Pépin et al., Phys. Rev. B 100(6), 060101 (2019). Copyright 2019 American Physical Society. (c) Transition from graphite to hexagonal diamond and cubic diamond under low pressure, and to the fullerene phase under moderate pressure and shear conditions. Reprinted with permission from Gao et al., Carbon 146, 364–368 (2019). Copyright 2019 Elsevier Ltd. (d) Moment magnitudes of acoustic emission events, pressure, strain, and stress vs time. Reprinted with permission from Wang et al., Sci. Adv. 3(7), e1601896 (2017). 2024 American Association for the Advancement of Science.
    • Table 1. Comparison of the subsystems and multi-anvil presses installed at SECUF.

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      Table 1. Comparison of the subsystems and multi-anvil presses installed at SECUF.

      SubsystemCapabilities and characteristics
      SEHPHT20 000 t belt-type apparatusP ≥ 20 GPa, V ≥ 1000 mm3, T ≥ 2500 K,Solid condition
      cylindrical chamber
      3000 t Kawai pressP ≥ 28 GPa, V ≥ 10 mm3, T ≥ 2500 K,Solid condition
      octahedral chamber
      1000 t DIA pressP ≥ 23 GPa, V ≥ 10 mm3, T ≥ 2500 K,
      octahedral chamber
      1000 t Kawai pressP ≥ 28 GPa, V ≥ 10 mm3, T ≥ 2500 K,
      octahedral chamber
      LEHPHTHundred milliliter volume pressP ≥ 0.5 GPa, V ≥ 100 ml, T ≥ 800 K,Liquid condition
      cylindrical chamber
      Microliter volume pressP ≥ 1.8 GPa, V ≥ 10 µl, T ≥ 1000 K,Liquid condition
      cylindrical chamber
      NHPRapid compression press10.2 GPa in 20 ms, V ≥ 10 mm3, T ≥ 1600 K,Temporal nonequilibrium
      octahedral chamber
      D-DIA press8 GPa with shear deformation, V ≥ 10 mm3,Spatial nonequilibrium
      T ≥ 1600 K, cubic chamber
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    Yufei Ge, Shuailing Ma, Cun You, Kuo Hu, Chuang Liu, Yixuan Wang, Xinglin Wang, Xinyang Li, Hongyu Li, Qiang Tao, Shuqing Jiang, Lu Wang, Hu Tang, Di Yao, Zhi He, Xinyi Yang, Zhaodong Liu, Qiang Zhou, Pinwen Zhu, Bo Zou, Bingbing Liu, Tian Cui. A distinctive HPHT platform with different types of large-volume press subsystems at SECUF[J]. Matter and Radiation at Extremes, 2024, 9(6): 063801

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    Paper Information

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    Received: Feb. 26, 2024

    Accepted: Aug. 3, 2024

    Published Online: Jan. 8, 2025

    The Author Email:

    DOI:10.1063/5.0205477

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