Journal of Inorganic Materials, Volume. 40, Issue 4, 405(2025)

Influence of Sintering Conditions on Preparation of Nearly Stoichiometric SiC Fibers with Highly Crystalline Microstructure

Yanzi GOU1, Weifeng KANG1, and Pengren WANG2
Author Affiliations
  • 11. Science and Technology on Advanced Ceramic Fibers and Composites Laboratory, College of Aerospace Science and Engineering, National University of Defense Technology, Changsha 410073, China
  • 22. Jiuquan Satellite Launch Center, Lanzhou 732750, China
  • show less
    References(38)

    [1] KANG W, CHEN J, ZHANG Y et al. SiC fibers with different diameters exhibiting excellent high-temperature resistance and oxidation resistance[J]. Journal of Materials Research and Technology, 1559(2023).

    [2] CHEN J, ZHANG Y, YAN D et al. Flexible ultrafine nearly stoichiometric polycrystalline SiC fibers with excellent oxidation resistance and superior thermal stability up to 1900 ℃[J]. Journal of the European Ceramic Society, 1938.

    [3] XIANG Y, WU S, YU J et al. Long-time oxidation behavior of the nearly stoichiometric polycrystal-line SiC fibers under air atmosphere at different temperatures[J]. Journal of the European Ceramic Society, 3569(2024).

    [4] SHAN J, MO G, SUN Q et al. Fabrication of SiC (OAl) and SiC (Al) fibers by melt-spinning, UV curing, thermolysis and sintering of photo-sensitive polyvinylaluminocarbosilane[J]. Journal of the European Ceramic Society, 3501(2024).

    [5] MORSCHER G N, HURST J, BREWER D. Intermediate- temperature stress rupture of a woven Hi-Nicalon, BN-interphase, SiC-matrix composite in air[J]. Journal of the American Ceramic Society, 1441(2000).

    [6] KATOH Y, SNEAD L L, HENAGER C H et al. Current status and critical issues for development of SiC composites for fusion applications[J]. Journal of Nuclear Materials, 659(2007).

    [7] PANAKARAJUPALLY R P, MIRZA F, EL RASSI J et al. Solid particle erosion behavior of melt-in-filtrated SiC/SiC ceramic matrix composites (CMCs) in a simulated turbine engine environ- ment[J]. Composites Part B: Engineering, 108860(2021).

    [8] ARREGUI-MENA J D, KOYANAGI T, CAKMAK E et al. Qualitative and quantitative analysis of neutron irradiation effects in SiC/SiC composites using X-ray computed tomography[J]. Composites Part B: Engineering, 109896(2022).

    [9] ZHANG S, GAO X, HAN X et al. Prediction of strength and constitutive response of SiC/SiC composites considering fiber failure[J]. Composites Part B: Engineering, 252(2019).

    [10] BHATT R, ELDRIDGE J. Heat treatment effects on microstructure and properties of CVI SiC/SiC composites with SylramicTM-iBN SiC fibers[J]. Journal of the European Ceramic Society, 2376(2023).

    [11] ZHAO Z, LIAO W, CHEN J et al. Advanced research on the preparation and application of carbide ceramic fibers[J]. Journal of Advanced Ceramics, 1291(2024).

    [12] LV X, YUE M, FENG X et al. Rare earth mono-silicates as oxidation resistant interphase for SiCf/SiC CMC: investigation of SiCf/Yb2SiO5 model composites[J]. Journal of Advanced Ceramics, 702(2022).

    [13] YAJIMA S, HASEGAWA Y, OKAMURA K et al. Development of high tensile strength silicon carbide fibre using an organosilicon polymer precursor[J]. Nature, 525(1978).

    [14] YAJIMA S, OKAMURA K, HAYASHI J et al. Synthesis of continuous SiC fibers with high tensile strength[J]. Journal of the American Ceramic Society, 324(1976).

    [15] KANG W, ZHANG Q, GOU Y. Fabrication of highly crystalline titanium-containing SiC fibers with different boron contents exhibiting excellent electromagnetic wave absorption[J]. Journal of Materials Science, 2739(2024).

    [16] ZHANG Q, CHEN T, KANG W et al. Synthesis of polytitanocarbosilane and preparation of Si-C-Ti-B fibers[J]. Processes, 1189(2023).

    [17] WU S, GOU Y, XIANG Y et al. Effect of long-time annealing at high temperature on the microstructure and mechanical properties of different types of SiC fibers[J]. Composites Part A: Applied Science and Manufacturing, 108291(2024).

    [18] GOU Y, KANG W, ZHANG Q. Preparation of nearly stoichiometric SiC(Ti) fibers with highly crystalline microstructure from polytitanocarbosilane[J]. Journal of Inorganic Materials, 1377(2024).

    [19] BUNSELL A R, PIANT A. A review of the development of three generations of small diameter silicon carbide fibres[J]. Journal of Materials Science, 823(2006).

    [20] WANG P, LIU F, WANG H et al. A review of third generation SiC fibers and SiCf/SiC composites[J]. Journal of Materials Science and Technology, 2743(2019).

    [21] SCHAWALLER D, CLAUSS B, BUCHMEISER M R. Ceramic filament fibers-a review[J]. Macromolecular Materials and Engineering, 502(2012).

    [22] ISHIKAWA T, KOHTOKU Y, KUMAGAWA K et al. High- strength alkali-resistant sintered SiC fibre stable to 2200 ℃[J]. Nature, 773.

    [23] TAKEDA M, SAEKI A, SAKAMOTO J I et al. Effect of hydrogen atmosphere on pyrolysis of cured polycarbosilane fibers[J]. Journal of the American Ceramic Society, 1063(2000).

    [24] BHATT R, SOLA F, EVANS L et al. Microstruc-tural, strength, and creep characterization of Sylramic™, Sylramic™-iBN and super Sylramic™-iBN SiC fibers[J]. Journal of the European Ceramic Society, 4697(2021).

    [25] ZHANG Y, WU C, WANG Y et al. A detailed study of the microstructure and thermal stability of typical SiC fibers[J]. Materials Characterization, 91(2018).

    [26] GOU Y, JIAN K, WANG H et al. Fabrication of nearly stoichiometric polycrystalline SiC fibers with excellent high-temperature stability up to 1900 ℃[J]. Journal of the American Ceramic Society, 2050.

    [27] WANG P, GOU Y, WANG H et al. Revealing the formation mechanism of the skin-core structure in nearly stoichiometric polycrystalline SiC fibers[J]. Journal of the European Ceramic Society, 2295(2020).

    [29] USUKAWA R, ODA H, ISHIKAWA T et al. Conversion process of amorphous Si-Al-C-O fiber into nearly stoichiometric SiC polycrystalline fiber[J]. Journal of the Korean Ceramic Society, 610(2016).

    [30] OKAMURA K, SHIMOO T, SUZUYA K et al. SiC-based ceramic fibers prepared via organic-to-inorganic conversion process-a review[J]. Journal of the Ceramic Society of Japan, 445(2006).

    [31] JACOBSON N S, KLINE S E. A thermoanalytical study of the conversion of amorphous Si-Ti-C-O fibers to SiC[J]. International Journal of Applied Ceramic Technology, 816(2012).

    [32] SNEAD L L, NOZAWA T, KATOH Y et al. Hand-book of SiC properties for fuel performance modeling[J]. Journal of Nuclear Materials, 329(2007).

    [33] VAN DER BERG N, MALHERBE J B, BOTHA A et al. Thermal etching of SiC[J]. Applied Surface Science, 5561(2012).

    [34] ZHANG Y, CHEN J, YAN D et al. Conversion of silicon carbide fibers to continuous graphene fibers by vacuum annealing[J]. Carbon, 435(2021).

    [35] ZHANG Y, CHEN T, CHEN J et al. The effects of annealing atmosphere and intrinsic component on high temperature evolution behaviors of SiC fibers[J]. Materials Science and Engineering: A, 143363(2022).

    [36] OKUMURA H, SAKUMA E, LEE J et al. Raman scattering of SiC: application to the identification of heteroepitaxy of SiC polytypes[J]. Journal of Applied Physics, 1134(1987).

    [37] DONG S, CHOLLON G, LABRUGERE C et al. Characterization of nearly stoichiometric SiC ceramic fibres[J]. Journal of Materials Science, 2371(2001).

    [38] LIPOWITZ J. Structure and properties of ceramic fibers prepared from organosilicon polymers[J]. Journal of Inorganic and Organometallic Polymers and Materials, 277(1991).

    Tools

    Get Citation

    Copy Citation Text

    Yanzi GOU, Weifeng KANG, Pengren WANG. Influence of Sintering Conditions on Preparation of Nearly Stoichiometric SiC Fibers with Highly Crystalline Microstructure[J]. Journal of Inorganic Materials, 2025, 40(4): 405

    Download Citation

    EndNote(RIS)BibTexPlain Text
    Save article for my favorites
    Paper Information

    Category:

    Received: Oct. 18, 2024

    Accepted: --

    Published Online: Sep. 2, 2025

    The Author Email:

    DOI:10.15541/jim20240439

    Topics