<trans-title>Synthesis of High Entropy Carbide Nano Powders <i>via</i> Liquid Polymer Precursor Route</trans-title>

Yanan SUN; Li YE; Wenying ZHAO; Fenghua CHEN; Wenfeng QIU; Weijian HAN; Wei LIU; Tong ZHAO

doi:10.15541/jim20200391

Journal of Inorganic Materials, Volume. 36, Issue 4, 393(2021)

Synthesis of High Entropy Carbide Nano Powders via Liquid Polymer Precursor Route

Yanan SUN1... Li YE1, Wenying ZHAO1, Fenghua CHEN1, Wenfeng QIU2, Weijian HAN1, Wei LIU and Tong ZHAO1,* |Show fewer author(s)

Author Affiliations

¹1. Key Laboratory of Science and Technology on High-tech Polymer Materials, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China

²2. South China Advanced Institute for Soft Matter Science and Technology, South China University of Technology, Guangzhou 510641, China

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Figures & Tables(9)

1. Photograph of PHEC

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2. FT-IR spectrum of PHEC

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3. ¹H NMR spectra of PHEC

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4. TGA curves of cured PHEC

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5. Characterization of pyrolysis process for PHEC

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6. Schematic diagram of pyrolysis process for PHEC and possible reactions

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7. SEM analyses of PHEC ceramic powders pyrolyzed at 1800 ℃

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8. TEM analyses of PHEC ceramic powders pyrolyzed at 1800 ℃

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Table 1. Metal content, yield and viscosity of PHEC
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Table 1. Metal content, yield and viscosity of PHEC
Item Metal content/wt% Yield/wt% Viscosity/(mPa∙s)
1 2
(Ti, Zr, Hf, Ta)C 28 28.6 150 162

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Yanan SUN, Li YE, Wenying ZHAO, Fenghua CHEN, Wenfeng QIU, Weijian HAN, Wei LIU, Tong ZHAO. Synthesis of High Entropy Carbide Nano Powders via Liquid Polymer Precursor Route[J]. Journal of Inorganic Materials, 2021, 36(4): 393

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