Acta Optica Sinica, Volume. 41, Issue 18, 1831001(2021)

Microstructure and Stress of Zr Thin Film Deposited by Pulsed DC Sputtering

Jingtao Zhu1,2, Sheng Guo1,2, Jiaoling Zhao2,3、*, Jiayi Zhang1,2, Hangyu Zhu1,2, and Jianda Shao2,3,4
Author Affiliations
  • 1School of Physics Science and Engineering, Tongji University, Shanghai 200092, China
  • 2Laboratory of Thin Film Optics, Shanghai Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, Shanghai 201800, China
  • 3Key Laboratory of Materials for High Power Laser, Shanghai Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, Shanghai 201800, China
  • 4Hangzhou Institute for Advanced Study, University of Chinese Academy of Sciences, Hangzhou, Zhejiang 310024, China
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    Thin film deposition is the core in the filter preparation process and its optimization is of great significance for the stability improvement of thin film filters. In this paper, a Zr thin film was deposited by pulsed direct current (DC) magnetron sputtering at different working pressures (0.05--1.0 Pa) of Ar. The surface of the thin film was measured by a Zygo interferometer and then the film stress was calculated. The microstructure changes of the thin film were characterized by an X-ray diffractometer and an atomic force microscope. The results show that the Zr thin film exhibits compressive stress when the working pressure is higher than 0.1 Pa, and the stress decreases slowly with the decrease in working pressure. Furthermore, when the pressure is 0.05 Pa, the film exhibits tensile stress. The variations in the phase structures and surface roughness are analyzed to further explain the generation mechanism for tensile stress. The results show that the main reason for the tensile stress forming is the microstructure change caused by plastic flow in the metal. Our study optimizes the deposition process in the preparation of low-stress and self-supporting Zr filters and has significant application value in extreme ultraviolet lithography, synchrotron radiation, and astronomical observation.

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    Jingtao Zhu, Sheng Guo, Jiaoling Zhao, Jiayi Zhang, Hangyu Zhu, Jianda Shao. Microstructure and Stress of Zr Thin Film Deposited by Pulsed DC Sputtering[J]. Acta Optica Sinica, 2021, 41(18): 1831001

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    Paper Information

    Category: Thin Films

    Received: Mar. 12, 2021

    Accepted: Apr. 7, 2021

    Published Online: Sep. 3, 2021

    The Author Email: Zhao Jiaoling (jolin923@siom.ac.cn)

    DOI:10.3788/AOS202141.1831001

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