The comprehensive experimental design takes the “flexible Zn-air battery” as the research and development hotspot. It relies on the major of new energy to solve the problems in the air cathode catalyst of flexible Zn-air battery. The axial coordination strategy is adopted to prepare the iron phthalocyanine (FePc) and the functional MXene composite catalytic materials. Besides, the physical characterization and electrochemical performance are conducted and further evaluated. This teaching design helps students master the basic preparation method of catalytic materials and deeply understand the electrochemical theory. It is also beneficial to make students be familiar with the assembly process and testing methods of flexible zinc-air batteries as well as the basic process of scientific research. Furthermore, the students can better understand the significance of new energy courses and improve the awareness of scientific research, exploration, and independent learning ability.