NUCLEAR TECHNIQUES, Volume. 48, Issue 5, 050601(2025)
Microstructure and mechanical properties of SiCf/SiC brazed joints
Continuous SiC fiber-reinforced SiC-matrix composites (SiCf/SiC) can be used as the fuel cladding, control rod sheath, intermediate heat exchanger, and tube components for nuclear reactor, the reliability of its joining is very crucial to the safety of nuclear energy.
This study aims to explore the microstructure and mechanical properties of SiCf/SiC brazed joints, and optimize processing of connecting SiCf/SiC with SiCf/SiC using brazing method.
SiCf/SiC was firstly prepared by chemical vapor infiltration (CVI) method, and active brazing method was used to join SiCf/SiC under 850 ℃, 870 ℃, and 890 ℃ with Ag-26.77Cu-4.4Ti (wt.%) filler metal. Then, the microstructure and interfacial phase of the brazed joint under different temperatures were analyzed for a high joining performance using optical microscopy (OM), scanning electron microscope (SEM), and energy dispersive spectrometer (EDS). The mechanical properties of the brazed joint were analyzed using thermal simulated test machine.
Observation results indicate that AgCuTi filler realizes stable joining for SiCf/SiC, and the surface smoothing of SiCf/SiC is beneficial to improve the shear strength of the joint. The reaction between Ti, Si, and C becomes more intense with the increase of the brazing temperature. When the brazing temperature reaches 890 °C, the brittle phase of Ti5Si3 gradually diffuses and disperses to the brazing seam, and the reinforced phase TiC becomes the main component of reaction layer, which effectively improves the microstructure and significantly increases the strength of the SiCf/SiC brazed joint.
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Baoliang ZHANG, Hongqiang ZHANG, Menghe TU, Yu ZHANG, Wei GUO. Microstructure and mechanical properties of SiCf/SiC brazed joints[J]. NUCLEAR TECHNIQUES, 2025, 48(5): 050601
Category: NUCLEAR ENERGY SCIENCE AND ENGINEERING
Received: May. 28, 2024
Accepted: --
Published Online: Jun. 26, 2025
The Author Email: ZHANG Hongqiang (张宏强)