NUCLEAR TECHNIQUES, Volume. 48, Issue 5, 050601(2025)

Microstructure and mechanical properties of SiCf/SiC brazed joints

Baoliang ZHANG1... Hongqiang ZHANG2,3,*, Menghe TU1, Yu ZHANG2, and Wei GUO23 |Show fewer author(s)
Author Affiliations
  • 1China Institute of Atomic Energy, Beijing 102413, China
  • 2Beihang University, Beijing 100083, China
  • 3Jiangxi Research Institute, Beihang University, Nanchang 330096, China
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    Background

    Continuous SiC fiber-reinforced SiC-matrix composites (SiCf/SiC) can be used as the fuel cladding, control rod sheath, intermediate heat exchanger, and tube components for nuclear reactor, the reliability of its joining is very crucial to the safety of nuclear energy.

    Purpose

    This study aims to explore the microstructure and mechanical properties of SiCf/SiC brazed joints, and optimize processing of connecting SiCf/SiC with SiCf/SiC using brazing method.

    Methods

    SiCf/SiC was firstly prepared by chemical vapor infiltration (CVI) method, and active brazing method was used to join SiCf/SiC under 850 ℃, 870 ℃, and 890 ℃ with Ag-26.77Cu-4.4Ti (wt.%) filler metal. Then, the microstructure and interfacial phase of the brazed joint under different temperatures were analyzed for a high joining performance using optical microscopy (OM), scanning electron microscope (SEM), and energy dispersive spectrometer (EDS). The mechanical properties of the brazed joint were analyzed using thermal simulated test machine.

    Results & Conclusions

    Observation results indicate that AgCuTi filler realizes stable joining for SiCf/SiC, and the surface smoothing of SiCf/SiC is beneficial to improve the shear strength of the joint. The reaction between Ti, Si, and C becomes more intense with the increase of the brazing temperature. When the brazing temperature reaches 890 °C, the brittle phase of Ti5Si3 gradually diffuses and disperses to the brazing seam, and the reinforced phase TiC becomes the main component of reaction layer, which effectively improves the microstructure and significantly increases the strength of the SiCf/SiC brazed joint.

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    Baoliang ZHANG, Hongqiang ZHANG, Menghe TU, Yu ZHANG, Wei GUO. Microstructure and mechanical properties of SiCf/SiC brazed joints[J]. NUCLEAR TECHNIQUES, 2025, 48(5): 050601

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    Paper Information

    Category: NUCLEAR ENERGY SCIENCE AND ENGINEERING

    Received: May. 28, 2024

    Accepted: --

    Published Online: Jun. 26, 2025

    The Author Email: ZHANG Hongqiang (张宏强)

    DOI:10.11889/j.0253-3219.2025.hjs.48.240227

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