Mass spectras of CS2, CH, and CH3OH were measured with a time-of-flight (TOF) under conditions with laser intensity varying from 1013 W/cm2 to 1016 W/cm2 and a pulse duration of 110 fs. Different mass spectras with linear polarization and circularly polarization were observed The angular distribution of ions of CS2 indicated a spatial alignment from the coulomb explosion of highly charged parent ion. Moreover, the comparision of mass spectra with CH4 and CH3OH does not exhibit a feature of the double peak splited from C ions, which manifestes a concerted explosive process of CH4 This is consistent with the results of CS2 analysed by the method of the kinetic energy release(KER).