Journal of Synthetic Crystals, Volume. 50, Issue 3, 435(2021)
Preparation and Properties of Transparent Eu∶Lu2O3 Scintillation Ceramics
The 5% Eu∶Lu2O3 ceramic precursor was synthesized by wet chemical method, and the morphologies, microstructures and phases of both Eu∶Lu2O3 ceramic precursor and the calcined Eu∶Lu2O3 ceramic powders were studied by SEM and XRD. The results show that the powders are spherical, well-dispersed and good crystalline. The particle size is calculated to be about 68.5 nm. Using the powders calcined at 1 100 ℃ for 4 h as raw material, the highly transparent Eu∶Lu2O3 ceramics were successfully fabricated by vacuum sintering at 1 650 ℃ for 30 h.The grain size is calculated to be about 46 μm, and in-line transmittance of the Eu∶Lu2O3 ceramics reaches 66.3% at 611 nm. What’s more, the absorption curve, the excitation spectrum, the emission spectrum and the X-ray excited emission spectrum of the Eu∶Lu2O3 ceramics were studied. It can be observed that the absorption curve of Eu∶Lu2O3 ceramics is consisted of the matrical absorption and active ion absorption. It can be seen from the photo-luminescence emission spectrum and X-ray excited emission spectrum of the Eu∶Lu2O3 ceramics that an extremely strong peak is located at 611 nm, corresponding to the 5D0→7F2 transition of Eu3+. By comparison with the BGO crystal, the light output of the Eu∶Lu2O3 ceramics is estimated to be about 85 000 ph/MeV. Eu∶Lu2O3 ceramics have an excellent X-ray stopping power due to its high density and effective atomic number. It is indicated that Eu∶Lu2O3 ceramics are a potential ceramic scintillator for the application of X-ray detection imaging combined with the characteristics of high light output.
Get Citation
Copy Citation Text
WANG Jing, GE Ye, XIE Weifeng, CHEN Haohong, LI Jiang. Preparation and Properties of Transparent Eu∶Lu2O3 Scintillation Ceramics[J]. Journal of Synthetic Crystals, 2021, 50(3): 435
Category:
Received: Dec. 14, 2020
Accepted: --
Published Online: Apr. 15, 2021
The Author Email:
CSTR:32186.14.