In order to rapidly prepare the filter media loaded with manganese oxide membrane, zeolite modified with sodium dodecyl sulfate (SLS) solution was used as the carrier, and the membrane hanging solution was used to rapidly load the manganese oxide membrane on the modified zeolite filter column, and the effects of the initial concentration and filtration rate on the effect of the column on the removal of NH₄⁺ and Mn²⁺ were investigated. The results showed that 200mg/L Mn²⁺ solution and 0.01 mol/L KMnO₄ solution were periodically run to dynamically load the membrane on the column, and the membrane was successfully loaded on the 7th day, and the concentrations of NH₄⁺ and Mn²⁺ in the effluent water were 0.199 mg/L and 0.066 mg/L, which were lower than the limit values of NH₄⁺ and Mn²⁺ in the "Hygiene Standard for Drinking Water" (GB 5749－2022). The removal rate of Mn²⁺ was 98.4%～96.7% when the concentration of NH₄⁺ inlet water was 2 mg/L, and 49.5% when the concentration of NH₄⁺ inlet water was 3～8 mg/L. The removal rate of Mn²⁺ was 97.6%～89.5% when the concentration of Mn²⁺ inlet water was 1～8 mg/L. The inhibition effect of initial concentration of NH₄⁺ on the removal of Mn²⁺ was significant, and the removal rate of Mn²⁺ was 0.066, 0.199, 0.066 mg/L, which was lower than that of NH₄⁺ and Mn²⁺ in GB 5749－2022. The initial concentration of NH₄⁺ had a significant inhibitory effect on the removal of Mn²⁺, and the initial concentration of Mn²⁺ had no effect on the removal of NH₄⁺. The effluent NH₄⁺ and Mn²⁺ concentrations were 0.25 mg/L and 0.088 mg/L, respectively, when the controlled filtration rate was 4 m/h. By comprehensive characterization of natural zeolite, modified zeolite, and membrane-hanging zeolite, the results showed that the modification of the natural zeolite by SLS was successful in improving the adsorption effect of the zeolite on Mn²⁺, and realizing a large amount of accumulation of Mn²⁺ on the surface of the zeolite. The main components of the manganese oxide film are Mn₃O₄ and MnO₂, which have oxidizing effects on NH₄⁺ and Mn²⁺.