[1] [1] ZHANG Y F, DING L, ZHAO W, et al. Hydrophobic bifunctionalized hexagonal mesoporous silicas as efficient adsorbents for the removal of orange IV［J］. RSC Advance, 2014, 4(91): 49783-49788.

[2] [2] KORENIUK A, MARESZ K, ODROZEK K, et al. Highly effective continuous-flow monolithic silica microreactors for acid catalyzed processes［J］. Applied Catalysis A: General, 2015, 489: 203-208.

[3] [3] LI J, LI L S, XU L. Hierarchically macro/mesoporous silica sphere: a high efficient carrier for enzyme immobilization［J］. Microporous and Mesoporous Materials, 2016, 231: 147-153.

[4] [4] SHI Z G, GUO Q Z, LIU Y T, et al. Drug delivery devices based on macroporous silica spheres［J］. Materials Chemistry and Physics, 2011, 126(3): 826-831.

[5] [5] JARAMILLO N, PAUCAR C, FERNNDEZ A, et al. Microemulsion assisted sol-gel method as approach to load a model anticancer drug inside silica nanoparticles for controlled release applications［J］. Colloid and Interface Science Communications, 2018, 24: 13-17.

[6] [6] HAN C L, HU Y P, WANG K, et al. Synthesis of mesoporous silica microspheres by a spray-assisted carbonation microreaction method［J］. Particuology, 2020, 50: 173-180.

[7] [7] ALONSO B, DOUY A, VRON E, et al. Morphological and textural control of spray-dried mesoporous silica-based spheres［J］. Journal of Materials Chemistry, 2004, 14(13): 2006-2016.

[8] [8] ZHOKHOV A A, MASALOV V M, SUKHININA N S, et al. Photonic crystal microspheres［J］. Optical Materials, 2015, 49: 208-212.

[9] [9] JIANG Z T, ZUO Y M. Synthesis of porous titania microspheres for HPLC packings by polymerization-induced colloid aggregation (PICA)［J］. Analytical Chemistry, 2001, 73(3): 686-688.

[10] [10] HE J L, CHEN X H, ZHU W J, et al. Preparation of porous silica microspheres by polymerization-induced colloid aggregation method［J］. Advanced Materials Research, 2014, 898: 132-135.

[11] [11] ARRIAGADA F J, OSSEO-ASARE K. Synthesis of nanosize silica in a nonionic water-in-oil microemulsion: effects of the water/surfactant molar ratio and ammonia concentration［J］. Journal of Colloid and Interface Science, 1999, 211(2): 210-220.

[12] [12] PENG R, KHAN M A, WU J, et al. In situ dielectric spectroscopy monitoring of silica nanoparticle synthesis in cationic water-in-oil microemulsions［J］. Langmuir, 2022, 38(13): 4121-4128.

[13] [13] HU Y N, HAO D X, GONG F L, et al. Facile one-pot emulsion/sol-gel method for preparing wrinkled silica microspheres［J］. Particuology, 2021, 56: 33-42.

[14] [14] ZHAO B B, ZHANG Y, TANG T, et al. Preparation of high-purity monodisperse silica microspheres by the sol-gel method coupled with polymerization-induced colloid aggregation［J］. Particuology, 2015, 22: 177-184.

[15] [15] KIM J W, SUH K D. Monodisperse polymer particles synthesized by seeded polymerization techniques［J］. Journal of Industrial and Engineering Chemistry, 2008, 14(1): 1-9.

[16] [16] STBER W, FINK A, BOHN E. Controlled growth of monodisperse silica spheres in the micron size range［J］. Journal of Colloid and Interface Science, 1968, 26(1): 62-69.

[17] [17] GAO W H, RIGOUT M, OWENS H. Facile control of silica nanoparticles using a novel solvent varying method for the fabrication of artificial opal photonic crystals［J］. Journal of Nanoparticle Research: an Interdisciplinary Forum for Nanoscale Science and Technology, 2016, 18(12): 387.

[18] [18] CHEN S L, YUAN G M, HU C T. Preparation and size determination of monodisperse silica microspheres for particle size certified reference materials［J］. Powder Technology, 2011, 207(1/2/3): 232-237.

[19] [19] QIU H D, LIANG X J, SUN M, et al. Development of silica-based stationary phases for high-performance liquid chromatography［J］. Analytical and Bioanalytical Chemistry, 2011, 399(10): 3307-3322.

[20] [20] VON HOHENESCHE C D F, EHWALD V, UNGER K K. Development of standard operation procedures for the manufacture of n-octadecyl bonded silicas as packing material in certified reference columns for reversed-phase liquid chromatography［J］. Journal of Chromatography A, 2004, 1025(2): 177-187.