Laser & Optoelectronics Progress, Volume. 61, Issue 3, 0314004(2024)

Metallurgical Defects, Microstructure, and Mechanical Properties of ECY768 Alloy Processed via Laser Powder Bed Fusion (Invited)

Haobo Liu1,2, Kaiwen Wei1、*, Qiao Zhong1, Jianqiang Gong1, Xiangyou Li1, and Xiaoyan Zeng1
Author Affiliations
  • 1Wuhan National Laboratory for Optoelectronics, Huazhong University of Science and Technology, Wuhan 430074, Hubei , China
  • 2Beijing Xinghang Electro-Mechnical Co., Ltd., Beijing 100074, China
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    Figures & Tables(21)
    ECY768 alloy powder. (a) Typical morphology; (b) particle-size distribution
    Illustration of grating type laser scanning strategy
    Tensile specimen blank and process test block. (a) Dimensional schematic; (b) photo of forming specimens
    Design dimensions of tensile specimens
    Process window for ECY768 alloy processed by LPBF
    Typical defect characteristics or appearance of representative specimens within different process windows (specimen numbers correspond to those in Fig. 5)
    Comparison of the morphology of pore defects before and after metallographic corrosion. (a) Nearly spherical pores; (b) irregular pores
    EDS and EBSD analysis of cracked regions. (a) EDS; (b) EBSD
    Effect law of process parameters on the porosity. (a) P=200 W, D=0.04 mm; (b) P=300 W, D=0.04 mm; (c) P=400 W, D=0.04 mm; (d) P=200 W, D=0.02 mm; (e) P= 300 W, D=0.02 mm
    Scatter plot of porosity and laser energy density. (a) Laser energy density of 26.04-312.50 J·mm-3; (b) laser energy density of 62.50-112.50 J·mm-3
    Scatter plot of crack rate and laser energy density. (a) Laser energy density of 26.04‒312.5 J·mm-3; (b) laser energy density of 26.04‒65.00 J·mm-3; (c) laser energy density of 125.00‒312.50 J·mm-3
    Optical micrographs of ECY768 alloy processed by LPBF after corrosion under the optimized processing parameters. (a) Vertical section; (b) horizontal section
    EBSD-IPF and EBSD-PF of ECY768 alloy processed by LPBF under the optimized processing parameters. (a) Vertical section; (b) horizontal section
    SEM images of microstructure in the grains of ECY768 alloy processed by LPBF under the optimized processing parameters. (a) (c) (e) Vertical sections; (b) (d) (f) horizontal sections
    X-ray diffraction spectra of ECY768 alloy processed by LPBF under the optimized processing parameters
    TEM analysis results of ECY768 alloy processed by LPBF under the optimized processing parameters. (a) HADDF image of sub-grain; (b) EDS maps for Co, Ni, Cr, Ta, Ti, and C elements; (c) HRTEM image of MC type carbide phase and its atomic arrangement along the [0 -1 1] crystal axis of the matrix; (d) HRTEM image of M23C6 type carbide phase and its atomic arrangement along the [0 -1 1] crystal axis of the matrix; (e) dislocation-carbide interactions
    Microhardness distribution of ECY768 alloy processed by LPBF under the optimized processing parameters
    Tensile engineering stress-strain curves at room temperature for ECY768 alloy processed by LPBF under the optimized processing parameters
    • Table 1. Elemental composition of ECY768 alloy powders

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      Table 1. Elemental composition of ECY768 alloy powders

      ElementCoCrNiWTaCFeTiAlOOther
      Mass fraction /%Bal.23.6410.467.073.520.570.340.280.180.0120.008
    • Table 2. Parameters for LPBF processing experiments

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      Table 2. Parameters for LPBF processing experiments

      Layer thickness /mmLaser power /WLaser scanning speed /(mm·s-1Hatch spacing /mmLaser defocus /mmRotation angle /(°)
      0.04200400‒16000.08‒0.12+2.590
      300
      400
      0.02200800‒14000.08‒0.12+2.590
      300
      400
    • Table 3. Room temperature tensile properties of ECY768 alloy processed by LPBF under the optimized processing parameters and their comparison with other main cobalt-based superalloys formed by LPBF or by casting

      View table

      Table 3. Room temperature tensile properties of ECY768 alloy processed by LPBF under the optimized processing parameters and their comparison with other main cobalt-based superalloys formed by LPBF or by casting

      Alloy stateDirectionUTS /MPaYS /MPaEL /%
      LPBF ECY768Parallel to build direction1467.1±18.71002.6±7.910.5±0.72
      Perpendicular to build direction1633.9±37.91267.9±62.413.3±0.35
      LPBF M-M5098Parallel to build direction139281710.8
      Perpendicular to build direction136510414.0

      LPBF M-M50910

      (carbon-free)

      Parallel to build direction100675410.4
      Perpendicular to build direction101266212.9
      LPBF K640S28Perpendicular to build direction87046214.5
      Cast M-M509297745203.4
      Cast K6402973542012.5
      Cast K6509267414805
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    Haobo Liu, Kaiwen Wei, Qiao Zhong, Jianqiang Gong, Xiangyou Li, Xiaoyan Zeng. Metallurgical Defects, Microstructure, and Mechanical Properties of ECY768 Alloy Processed via Laser Powder Bed Fusion (Invited)[J]. Laser & Optoelectronics Progress, 2024, 61(3): 0314004

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    Paper Information

    Category: Lasers and Laser Optics

    Received: Sep. 25, 2023

    Accepted: Nov. 27, 2023

    Published Online: Mar. 7, 2024

    The Author Email: Wei Kaiwen (Laser_wei@hust.edu.cn)

    DOI:10.3788/LOP232185

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