Spectroscopy and Spectral Analysis, Volume. 42, Issue 2, 415(2022)

Characterization of Moisture Absorption Process of Stevia and Rapid Determination of Rebaudioside a Content by Using Near-Infrared Spectroscopy

Figures & Tables(9)
Moisture absorption curve of stevia
Spectral changes of stevia during moisture absorption(a): Raw spectra; (b): Multivariate scatter correction spectra;(c): A magnified plot at 1 850~2 050 nm; (d): Second derivative spectra of 1 850~2 050 nm
Spectra of 55 stevia samples with different RA content(a): Raw spectra; (b): Spectra after MSC processing
Scores and loadings of the first two principal components in the combination bands of OH in the moisture absorption process(a): Scores of the first principal component; (b): Loadings of the first principal component;(c): Scores of the second principal component; (d): Loadings of the second principal component
Synchronous (1) and asynchronous (2) 2D correlation spectra of the stevia moisture absorption processThe first hour (a1, a2) the middle two hours (b1, b2) and the last hour (c1, c2)
Schematic diagram of the calculation process of the EPO algorithm(a): The spectra before EPO correction; (b): The difference spectra of the stevia moisture absorption process;(c): The cross-validation error graph generated by different combinations of c and LVs; (d): The spectra after EPO correction
(a) LV-RMSECV curve; (b) NIRS quantitative analysis model of RA content in stevia
  • Table 1. Moisture absorption kinetic model of stevia

    View table
    View in Article

    Table 1. Moisture absorption kinetic model of stevia

    样品吸湿方程R2吸湿速度方程吸湿初始速度
    /(%·min-1)
    吸湿加速度
    /(%·min-1)
    吸湿平衡
    时间/min
    平衡含水
    率/%
    甜菊糖y=-0.000 2t2+0.076 4t+0.242 20.990 2v=-0.000 4t+0.076 40.076 4-0.000 41917.538
  • Table 2. External test sets results of RA's NIRS quantitative analysis model

    View table
    View in Article

    Table 2. External test sets results of RA's NIRS quantitative analysis model

    样本信息None-EPO+MSCEPO+MSC
    预测值/%误差/%预测值/%误差/%
    1#(90.27%)98.468.1991.491.22
    2#(92.90%)98.805.9092.440.46
    3#(95.32%)101.025.7095.610.29
    4#(97.16%)101.274.1197.070.09
    5#(98.23%)103.184.9598.190.04
    平均误差/%5.770 60.420 1
    RMSEP/%6.629 10.669 5
    RP20.896 90.957 0
    RPD0.293 14.336 8
Tools

Get Citation

Copy Citation Text

. Characterization of Moisture Absorption Process of Stevia and Rapid Determination of Rebaudioside a Content by Using Near-Infrared Spectroscopy[J]. Spectroscopy and Spectral Analysis, 2022, 42(2): 415

Download Citation

EndNote(RIS)BibTexPlain Text
Save article for my favorites
Paper Information

Category: Research Articles

Received: Dec. 24, 2020

Accepted: Mar. 12, 2021

Published Online: Apr. 2, 2022

The Author Email:

DOI:10.3964/j.issn.1000-0593(2022)02-0415-08

Topics