Acta Photonica Sinica, Volume. 49, Issue 12, 216(2020)

Development of Polycarbonate High Strength Ultra-low Reflectivity Film

Dong-mei LIU1... Bo-yang WEI1,*, Xiu-hua FU1, Jing ZHANG1, Suo-tao DONG1 and Shuang LI2 |Show fewer author(s)
Author Affiliations
  • 1College of Photoelectric Engineering, Changchun University of Science and Technology, Changchun30022, China
  • 2Optorun (Shanghai) Co., Ltd., Shanghai00444,China
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    Figures & Tables(16)
    Refractive index of two materials
    Theoretical design curve of antireflection film
    Surface roughness of substrate at different plasma treatment times
    The surface roughness of the substrate during different plasma treatment times
    Stress fitting curve
    Spectral test curve
    Rate change curve
    Schematic diagram of PID control electron gun current
    Deposition rate after PID adjustment
    PID stable film forming rate spectral test curve
    • Table 1. Technical indexes of subtracting the reverse membrane

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      Table 1. Technical indexes of subtracting the reverse membrane

      ParametersIndicators
      SubstratePolycarbonate
      Incident angle/(º)0
      Spectral range/nm430~700
      Absolute reflectivity/%<0.15
    • Table 2. Polycarbonate synthesis and performance

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      Table 2. Polycarbonate synthesis and performance

      PerformanceNumerical
      Bibulous rate/%0.15
      Modulus of elasticity in tension/MPa2 200~2 500
      Bending strength/MPa106
      Coefficient of linear expansion/(10-5K-1)6~7
      Brinell hardness/MPa97~104
      Transmittance magnitude/%87~90
    • Table 3. Vacuum cooling parameters

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      Table 3. Vacuum cooling parameters

      Annealing

      temperature/℃

      Annealing time/hIon source energyFilm stress/MPa
      Voltage/VCurrent/mAAnnealing beforeAfter annealing
      Sample11201300300-265-205
      Sample21202300300-253-213
      Sample31203300300-256-209
      Sample41204300300-258-224
    • Table 4. Monolayer stress of the two materials

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      Table 4. Monolayer stress of the two materials

      Deposition time/sSingle layer stress/MPa
      TiO2SiO2
      30-426-476
      60-455-477
      90-484-398
    • Table 5. Notched ion source process parameters record table

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      Table 5. Notched ion source process parameters record table

      Membrane layerMaterialVoltage/VCurrent/mAAcc/VO2/sccmAr/sccm
      1~2TiO28008001509010
      SiO2800800150608
      3~8TiO25005001509010
      SiO2500500150608
      TiO25005001509010
      SiO2500500150608
      TiO25005001509010
      SiO2500500150608
      9~10TiO28008001509010
      SiO2800800150608
    • Table 6. Layered gradient stress of anti-reflection film

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      Table 6. Layered gradient stress of anti-reflection film

      Membrane layerStress/MPa
      1~2-132
      1~8-84
      1~10-96
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    Dong-mei LIU, Bo-yang WEI, Xiu-hua FU, Jing ZHANG, Suo-tao DONG, Shuang LI. Development of Polycarbonate High Strength Ultra-low Reflectivity Film[J]. Acta Photonica Sinica, 2020, 49(12): 216

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    Paper Information

    Category: Thin Films

    Received: --

    Accepted: --

    Published Online: Mar. 11, 2021

    The Author Email: WEI Bo-yang (2824155502@qq.com)

    DOI:10.3788/gzxb20204912.1231001

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