Acta Optica Sinica, Volume. 43, Issue 11, 1134001(2023)

Preparation of X-Ray Fresnel Zone Plate by Atomic Layer Deposition and Focused Ion Beam Slicing

Mingsheng Tan1,3, Shuaiqiang Ming1, Yufei Wu1,3, Weier Lu1,3、*, Yanli Li2、**, Xiangdong Kong2,3、***, Haigang Liu4, Yang Xia1,3, and Li Han2,3
Author Affiliations
  • 1Institute of Microelectronics, Chinese Academy of Sciences, Beijing 100029, China
  • 2Institute of Electrical Engineering, Chinese Academy of Sciences, Beijing 100190, China
  • 3University of Chinese Academy of Sciences, Beijing 100049, China
  • 4Shanghai Synchrotron Radiation Facility, Shanghai Advanced Research Institute, Chinese Academy of Sciences, Shanghai 201800, China
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    Figures & Tables(9)
    Structural design of X-ray zone plate. (a) Structure diagram of zone plate; (b) variation of diffraction efficiency of Al2O3/HfO2 zone plate with thickness at 1.2 keV
    Process roadmap for preparing X-ray multilayer zone plates
    Ellipsometer test results of Al2O3 and HfO2 film thickness
    Rate correction result diagram. (a) SEM images of multilayer films on Si slices; (b) the comparison curve between theoretical and measured film thickness
    SEM images of FIB slicing process and prepared zone plate. (a) Cutting; (b) extraction; (c) transfer and fixation; (d) top view; (e) sectional view; (f) partial enlarged view
    Partial enlarged SEM images of defects in multilayer zone plates. (a) Crack through the whole zone part; (b) interfacial crack between multilayers and substrate; (c) crack in the outer zones
    Imaging testing of X-ray zone plates. (a) Schematic diagram of test optical path; (b) SEM of gold plated star type standard target samples; (c) standard target center inner ring SEM enlarged view; (d) an optical microscope image of a zone plate fixed to a test optical path bracket; (e)(f) focused imaging of a star type standard target sample using a zone plate
    • Table 1. Structural design parameters of X-ray zone plate

      View table

      Table 1. Structural design parameters of X-ray zone plate

      X-ray energy

      E /keV

      Diameter of zone plate D /μmDiameter of central substrate d /μmOutermost zone width ΔrN /nmThickness of zone plate t /μm

      Focal length

      f /mm

      Number of zones

      n

      1.29272251.12.23356
    • Table 2. Test data of typical multilayer films

      View table

      Table 2. Test data of typical multilayer films

      Zone numberMeasured t1 /nmMeasured t2 /nmMeasured t3 /nmMeasured t4 /nmMeasured t5 /nmAverage t /nmStandard error /nmTheoretical t /nm
      4031.2031.0231.6631.1231.4631.290.2630.84
      8030.5529.3530.4129.6530.5530.100.5629.87
      12029.6228.4328.7829.1028.7628.940.4528.98
      16028.6827.2228.1027.8828.1228.000.5328.17
      20027.9027.2227.8828.0227.3227.670.3727.43
      24027.1226.9427.2526.8027.3027.100.2126.74
      28026.9825.6725.9826.3226.1026.210.4926.10
      32025.6224.9625.2025.4525.0725.260.2725.50
      36025.5624.8625.2324.9225.4825.210.3225.02
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    Mingsheng Tan, Shuaiqiang Ming, Yufei Wu, Weier Lu, Yanli Li, Xiangdong Kong, Haigang Liu, Yang Xia, Li Han. Preparation of X-Ray Fresnel Zone Plate by Atomic Layer Deposition and Focused Ion Beam Slicing[J]. Acta Optica Sinica, 2023, 43(11): 1134001

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    Paper Information

    Category: X-Ray Optics

    Received: Nov. 25, 2022

    Accepted: Feb. 21, 2023

    Published Online: May. 29, 2023

    The Author Email: Lu Weier (luweier@ime.ac.cn), Li Yanli (liyanli@mail.iee.ac.cn), Kong Xiangdong (slkongxd@mail.iee.ac.cn)

    DOI:10.3788/AOS222052

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