Acta Optica Sinica, Volume. 43, Issue 11, 1134001(2023)
Preparation of X-Ray Fresnel Zone Plate by Atomic Layer Deposition and Focused Ion Beam Slicing
Fig. 1. Structural design of X-ray zone plate. (a) Structure diagram of zone plate; (b) variation of diffraction efficiency of Al2O3/HfO2 zone plate with thickness at 1.2 keV
Fig. 2. Process roadmap for preparing X-ray multilayer zone plates
Fig. 3. Ellipsometer test results of Al2O3 and HfO2 film thickness
Fig. 4. Rate correction result diagram. (a) SEM images of multilayer films on Si slices; (b) the comparison curve between theoretical and measured film thickness
Fig. 5. SEM images of FIB slicing process and prepared zone plate. (a) Cutting; (b) extraction; (c) transfer and fixation; (d) top view; (e) sectional view; (f) partial enlarged view
Fig. 6. Partial enlarged SEM images of defects in multilayer zone plates. (a) Crack through the whole zone part; (b) interfacial crack between multilayers and substrate; (c) crack in the outer zones
Fig. 7. Imaging testing of X-ray zone plates. (a) Schematic diagram of test optical path; (b) SEM of gold plated star type standard target samples; (c) standard target center inner ring SEM enlarged view; (d) an optical microscope image of a zone plate fixed to a test optical path bracket; (e)(f) focused imaging of a star type standard target sample using a zone plate
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Mingsheng Tan, Shuaiqiang Ming, Yufei Wu, Weier Lu, Yanli Li, Xiangdong Kong, Haigang Liu, Yang Xia, Li Han. Preparation of X-Ray Fresnel Zone Plate by Atomic Layer Deposition and Focused Ion Beam Slicing[J]. Acta Optica Sinica, 2023, 43(11): 1134001
Category: X-Ray Optics
Received: Nov. 25, 2022
Accepted: Feb. 21, 2023
Published Online: May. 29, 2023
The Author Email: Lu Weier (luweier@ime.ac.cn), Li Yanli (liyanli@mail.iee.ac.cn), Kong Xiangdong (slkongxd@mail.iee.ac.cn)