Journal of Inorganic Materials, Volume. 37, Issue 7, 750(2022)

Preparation of SiO2@Ag@SiO2@TiO2 Core-shell Structure and Its Photocatalytic Degradation Property

Congcong CHI... Panpan QU, Chaonan REN, Xin XU, Feifei BAI and Danjie ZHANG |Show fewer author(s)
Author Affiliations
  • National Demonstration Center for Experimental Light Chemistry Engineering Education, Shaanxi Province Key Laboratory of Papermaking Technology and Specialty Paper, Key Laboratory of Paper based Functional Materials of China National Light Industry, Key Laboratory of Functional Printing and Transport Packaging of China National Light Industry, Shaanxi University of Science & Technology, Xi'an 710021, China
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    Figures & Tables(12)
    Schematic diagram for synthesizing SiO2@Ag@SiO2@TiO2 microspheres
    SEM images of SiO2@Ag microspheres prepared with different AgNO3/SiO2 mass ratios
    STEM image (a), EDS pattern of selected region (b), TEM image (c), and HRTEM image (d) of SiO2@Ag microspheres
    SEM images of SiO2@Ag microspheres before (a) and after (b) thermal-treated at 500 ℃
    SEM images of SiO2@Ag@SiO2 microspheres prepared with different TEOS/SiO2 mass ratios
    SEM images of SiO2@Ag@TiO2 microspheres with different TBOT/SiO2 mass ratios
    (a) TEM image, (b) EDS pattern, (c) HRTEM image and corresponding elemental mapping of O, Si, Ag and Ti of SiO2@Ag@SiO2@TiO2 microspheres
    XRD patterns of different SiO2-based microspheres
    Nitrogen adsorption-desorption isotherms of different SiO2-based microspheres
    ln(At/A0)-t curves of different samples and cyclic tests of MB degradation by SiO2@Ag@SiO2@TiO2 (insert)
    Transient photocurrent responses (a) and electrochemical impedance spectra (b) of different samples
    • Table 1. Pore structure parameters of different microspheres

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      Table 1. Pore structure parameters of different microspheres

      SampleSBET/ (m2·g-1) Pore volume/ (cm3·g-1) Average pore size/nm
      SiO218.950.2356.20
      SiO2@Ag 23.870.3862.78
      SiO2@Ag@TiO248.360.2315.85
      SiO2@Ag@SiO2@TiO281.360.2510.37
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    Congcong CHI, Panpan QU, Chaonan REN, Xin XU, Feifei BAI, Danjie ZHANG. Preparation of SiO2@Ag@SiO2@TiO2 Core-shell Structure and Its Photocatalytic Degradation Property [J]. Journal of Inorganic Materials, 2022, 37(7): 750

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    Paper Information

    Category: RESEARCH ARTICLE

    Received: Nov. 8, 2021

    Accepted: --

    Published Online: Jan. 10, 2023

    The Author Email:

    DOI:10.15541/jim20210685

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