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Journal of Inorganic Materials, Volume. 34, Issue 7, 761(2019)

Strontium Hydroxystannate Nanorods Encapsulated by Hybrid Polyphosphazene: Synthesis and Flame Retardancy on Epoxy Resin

Chong ZHANG1... Xiao-Wei GENG1, Xiang-Di GAO1, Xin ZHANG1, Rao GUO1, Yu-Jing WANG1, Jian-Zhong XU1, and Hai-Yun MA12,* |Show fewer author(s)
Author Affiliations
  • 1School of Chemistry and Environmental Sciences, Hebei University, Baoding 071002, China
  • 2Key Laboratory of Analytical Science and Technology of Hebei Province, Hebei University, Baoding 071002, China
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    AbstractGet PDF(in Chinese)
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    Figures & Tables(10)
    Synthetic routes of the SrSn(OH)6 and PZS@SrSn(OH)6
    1. Synthetic routes of the SrSn(OH)6 and PZS@SrSn(OH)6

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    Morphologies and element distribution map of SrSn(OH)6 and PZS@SrSn(OH)6
    2. Morphologies and element distribution map of SrSn(OH)6 and PZS@SrSn(OH)6

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    TG (a) and DTG (b) curves of SrSn(OH)6, PZS and PZS@SrSn(OH)6 tested in N2 atmosphere
    3. TG (a) and DTG (b) curves of SrSn(OH)6, PZS and PZS@SrSn(OH)6 tested in N2 atmosphere

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    TG (a) and DTG (b) curves of EP nanocomposites tested in N2 atmosphere
    4. TG (a) and DTG (b) curves of EP nanocomposites tested in N2 atmosphere

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    LOI values and residue chars at the end of LOI tests of EP, EP/SrSn(OH)6 and EP/PZS@SrSn(OH)6 nanocomposites
    5. LOI values and residue chars at the end of LOI tests of EP, EP/SrSn(OH)6 and EP/PZS@SrSn(OH)6 nanocomposites

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    Heat release rate (HRR) (a), specimen mass (b), smoke production rate SPR (c), and CO production rate (d) curves of the samples in CONE tests
    6. Heat release rate (HRR) (a), specimen mass (b), smoke production rate SPR (c), and CO production rate (d) curves of the samples in CONE tests

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    Digital photos of the char residues for composites after cone calorimeter tests
    7. Digital photos of the char residues for composites after cone calorimeter tests

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    XRD (a), EDS (b) and FT-IR (c) spectra of the char residue of EP samples
    8. XRD (a), EDS (b) and FT-IR (c) spectra of the char residue of EP samples

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    • Table 1. Thermogravimetric properties of PZS, SrSn(OH)6, PZS@SrSn(OH)6 and EP nanocomposites

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      Table 1. Thermogravimetric properties of PZS, SrSn(OH)6, PZS@SrSn(OH)6 and EP nanocomposites

      SampleT5%/℃Tmax/℃Residue at 800 ℃/wt%Theoretical residue at 800 ℃/wt%
      PZS442.8507.948.2—
      SrSn(OH)6217.3237.780.4—
      PZS@SrSn(OH)6218.5487.569.4—
      Pure EP364.2375.313.0—
      3% EP/SrSn(OH)6354.0367.316.215.0
      3% EP/PZS@SrSn(OH)6360.0368.617.014.7

    • Table 2. Cone calorimetry data for EP composites

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      Table 2. Cone calorimetry data for EP composites

      SamplePure EP1wt% EP/SrSn(OH)63wt% EP/SrSn(OH)61wt% EP/PZS@SrSn(OH)63wt% EP/PZS@SrSn(OH)6
      Char residue/g5.613.212.413.819.2
      THR/(MJ·m-2)100.493.292.693.188.9
      PHRR/(kW·m-2)1141.1971.7888.9777.3809.7
      PSPR/(m2·s)0.330.250.240.220.21
      TSP/m227.623.723.925.121.2
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    Chong ZHANG, Xiao-Wei GENG, Xiang-Di GAO, Xin ZHANG, Rao GUO, Yu-Jing WANG, Jian-Zhong XU, Hai-Yun MA. Strontium Hydroxystannate Nanorods Encapsulated by Hybrid Polyphosphazene: Synthesis and Flame Retardancy on Epoxy Resin[J]. Journal of Inorganic Materials, 2019, 34(7): 761

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    Paper Information

    Category: RESEARCH PAPER

    Received: Oct. 17, 2018

    Accepted: --

    Published Online: Sep. 26, 2021

    The Author Email: MA Hai-Yun (coffee1123@126.com)

    DOI:10.15541/jim20180493

    Topics

    laser devices and laser physics
    Lasers and Laser Optics
    Laser physics
    laser manufacturing
    Instrumentation, Measurement and Metrology