Journal of Inorganic Materials, Volume. 34, Issue 7, 755(2019)

Synthesis of Metastable Vaterite Phase of CaCO3via Ethanol-calcium Method and Ethanol-water Binary Solvent Method

Chuan-Jie CHEN1... Li-Geng WEI1, Yue WU1, Cheng-Pei HU1, Yuan-Cong HU1, and Jiu-Xin JIANG1,23,* |Show fewer author(s)
Author Affiliations
  • 1Hubei Provincial Key Laboratory of Green Materials for Light Industry, Hubei University of Technology, Wuhan 430068, China
  • 2Collaborative Innovation Center of Green Light-weight Materials and Processing, Hubei University of Technology, Wuhan 430068, China
  • 3School of Material and Chemistry Engineering, Hubei University of Technology, Wuhan 430068, China
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    Figures & Tables(6)
    XRD patterns of CaCO3 prepared from ethanol-calcium method (a-e) and EWBS method (f-j) after aging for different time
    SEM images of CaCO3 prepared from ethanol-calcium method (a-d) and EWBS method (e-h) after aging for different times
    XRD patterns of CaCO3 prepared from ethanol-calcium method (a-e) and EWBS method (f-j) at different reaction temperatures
    SEM images of CaCO3 prepared from ethanol-calcium method (a-e) and EWBS method (f-j) at different reaction temperatures
    The reaction process of ethanol-calcium method
    • Table 1. Phase compositions of CaCO3 prepared at different conditions

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      Table 1. Phase compositions of CaCO3 prepared at different conditions

      Aging time/minTemperature/℃*Polymorphs/%**Polymorphs/%
      VateriteCalciteVateriteCalcite
      02090.49.646.553.5
      202084.415.612.387.7
      902083.515.910.589.5
      13202082.517.50100
      25202081.418.60100
      60/10#085.814.257.142.9
      60/10#2084.115.944.355.7
      60/10#4073.326.722.677.4
      60/10#6070.229.80100
      60/10#8064.835.20100
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    Chuan-Jie CHEN, Li-Geng WEI, Yue WU, Cheng-Pei HU, Yuan-Cong HU, Jiu-Xin JIANG. Synthesis of Metastable Vaterite Phase of CaCO3via Ethanol-calcium Method and Ethanol-water Binary Solvent Method[J]. Journal of Inorganic Materials, 2019, 34(7): 755

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    Paper Information

    Category: RESEARCH PAPER

    Received: Oct. 10, 2018

    Accepted: --

    Published Online: Sep. 26, 2021

    The Author Email: JIANG Jiu-Xin (jiuxinjiang@hotmail.com)

    DOI:10.15541/jim20180472

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