NUCLEAR TECHNIQUES, Volume. 47, Issue 2, 020605(2024)

Effects of spark plasma sintering parameters on mechanical and thermal properties of U3Si2 pellets

Jinzhao ZOU1,3, Shizhuan XU1,3, Peng WANG1、**, Changqing CAO1, Chao YAN1, Zhiyong ZHU1, Jun LIN1、*, Yan YOU2, Junqiang LU2, and Libing ZHU2
Author Affiliations
  • 1Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800, China
  • 2Shanghai Nuclear Engineering Research and Design Institute Co., Ltd., Shanghai 200233, China
  • 3University of Chinese Academy of Sciences, Beijing 100049, China
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    Figures & Tables(7)
    Temperature dependence of the thermal diffusivity (a, b) and thermal conductivity (c, d) of U3Si2 pellets in the range 27~700 ℃
    SEM images of the indentations on the surfaces of the U3Si2 pellets (a) SPS-4 with plastic deformation, (b) SPS-4 with brittle fracture, (c) SPS-1 with brittle fracture, (d) testing area of SPS-5
    Hardness of U3Si2 pellets versus the indentation depth (a) 4 pellets prepared under different dwell temperatures at 60 MPa, (b) 2 pellets prepared under different pressures at 1 100 ℃, (c⁓h) H2-1/h curves of 6 U3Si2 pellets corresponding to (a) and (b)
    Hardness and fracture toughness of U3Si2 pellets against dwell temperature (a) and pressure (b), Young's modulus of the pellets against dwell temperature (c) and pressure (d)
    • Table 1. SPS parameters for U3Si2 pellets

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      Table 1. SPS parameters for U3Si2 pellets

      样品Samples

      SPS温度

      SPS temperature / ℃

      SPS压力

      SPS pressure / MPa

      SPS-11 00060
      SPS-21 10060
      SPS-31 20060
      SPS-41 30060

      SPS-5

      SPS-6

      1 100

      1 100

      30

      90

    • Table 2. Densities of SPS-fabricated U3Si2 pellets

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      Table 2. Densities of SPS-fabricated U3Si2 pellets

      样品

      Samples

      密度

      Density / g·cm-3

      相对密度

      Theoretical density / %

      SPS-111.4±0.1093.4
      SPS-211.6±0.0295.1
      SPS-311.9±0.0297.5
      SPS-412.0±0.0298.4

      SPS-5

      SPS-6

      10.6±0.40

      11.7±0.02

      86.9

      95.9

    • Table 3. (E/H)0.5 values of U3Si2 pellets and the average crack length under the HL mode of nanoindentation

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      Table 3. (E/H)0.5 values of U3Si2 pellets and the average crack length under the HL mode of nanoindentation

      样品

      Samples

      (E/H)0.5

      平均裂纹长度

      Average crack length / μm

      SPS-14.57.8±2.8
      SPS-24.49.6±2.0
      SPS-34.413.2±1.7
      SPS-44.515.0±1.6

      SPS-5

      SPS-6

      4.2

      4.3

      9.7±2.2

      8.3±2.2

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    Jinzhao ZOU, Shizhuan XU, Peng WANG, Changqing CAO, Chao YAN, Zhiyong ZHU, Jun LIN, Yan YOU, Junqiang LU, Libing ZHU. Effects of spark plasma sintering parameters on mechanical and thermal properties of U3Si2 pellets[J]. NUCLEAR TECHNIQUES, 2024, 47(2): 020605

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    Paper Information

    Category: Research Articles

    Received: Aug. 30, 2023

    Accepted: --

    Published Online: Apr. 24, 2024

    The Author Email: WANG Peng (王鹏), LIN Jun (林俊)

    DOI:10.11889/j.0253-3219.2024.hjs.47.020605

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