Spectroscopy and Spectral Analysis, Volume. 42, Issue 2, 603(2022)

Quantitative Analysis of Nickel-Based Superalloys Based on a Remote LIBS System

Figures & Tables(12)
Optical structure diagram of remote LIBS system
The best D1, D2 at different working distances
DOF at 5 m working distance
The Variation of DOF with working distance
LIBS spectra at different working distances
Variation of spectral line intensity with working distance
Focal spot at 2 m (a), 4 m (b), 6 m (c), 8 m (d)
The relationship between focal spot diameter and working distance
The standard curves of Ni (a, b), Cr (c, d), Nb (e, f), Mo (g, h), Ti (h, i) and Al (j, k)
The relationship between LIBS test result error and test times
  • Table 1. Standard values of GH4169 reference materials

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    Table 1. Standard values of GH4169 reference materials

    NumberNiCrMoNbAlTi
    GBW01008143.8922.214.036.790.681.42
    GBW01008248.6020.143.576.060.621.21
    GBW01008352.4718.463.085.150.410.94
    GBW01008456.6716.862.704.510.310.75
    GBW01008560.0014.872.293.850.140.59
    YSBS41503—201252.2718.563.285.150.6351.03
  • Table 2. Comparison of analysis results between remote LIBS and XRF

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    Table 2. Comparison of analysis results between remote LIBS and XRF

    ElementsMethodsw/%Average/%RE/%RSD/%
    NiLIBS
    XRF
    51.06, 52.67, 52.47, 52.17, 53.23, 50.96
    51.07, 51.10, 51.01, 51.16, 51.13, 51.09
    52.09
    51.09
    0.34
    2.25
    1.74
    0.10
    CrLIBS
    XRF
    17.95, 18.46, 17.78, 18.51, 19.28, 18.36
    18.45, 18.52, 18.49, 18.37, 18.35, 18.34
    18.39
    18.42
    0.92
    0.76
    2.85
    0.43
    NbLIBS
    XRF
    5.46, 4.96, 5.03, 5.24, 5.06, 5.21
    5.12, 5.07, 5.15, 5.11, 5.12, 5.10
    5.16
    5.11
    0.21
    0.72
    3.51
    0.49
    MoLIBS
    XRF
    3.16, 3.34, 3.07, 3.34, 3.41, 3.23
    3.27, 3.24, 3.27, 3.24, 3.27, 3.27
    3.26
    3.26
    0.68
    0.64
    3.90
    0.52
    TiLIBS
    XRF
    1.09, 0.93, 0.96, 1.03, 0.98, 1.02
    0.97, 0.99, 1.01, 0.96, 0.96, 1.00
    1.00
    0.98
    2.75
    4.68
    5.58
    2.39
    AlLIBS
    XRF
    0.59, 0.64, 0.58, 0.62, 0.64, 0.63
    0.63, 0.59, 0.61, 0.65, 0.58, 0.66
    0.62
    0.62
    2.93
    2.39
    4.15
    5.02
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. Quantitative Analysis of Nickel-Based Superalloys Based on a Remote LIBS System[J]. Spectroscopy and Spectral Analysis, 2022, 42(2): 603

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Paper Information

Category: Research Articles

Received: Jan. 6, 2021

Accepted: Feb. 1, 2021

Published Online: Apr. 2, 2022

The Author Email:

DOI:10.3964/j.issn.1000-0593(2022)02-0603-06

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