Spectroscopy and Spectral Analysis, Volume. 40, Issue 11, 3606(2020)

Two-Dimensional Perturbation Correlation Infrared Spectroscopy Analysis of Animal Manure Biochar

Xiang-yang GUI1...1,*, Chen LIU1,1, Ji-hong XU1,1, Fang-lei DUAN1,1, Shu-wei FANG1,1, and Fei-yue LI11 |Show fewer author(s)
Author Affiliations
  • 1[in Chinese]
  • 11. College of Resource and Environment, Anhui Science and Technology University, Fengyang 233100, China
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    Figures & Tables(6)
    Infrared spectra of biochars(a): Chicken manure; (b): Dairy manure; (c): Pig manure
    Correlation spectra of biochars in 3 600~2 800 cm-1 band(a): Chicken manure biochar; (b): Cow dung biochar; (c): Pig manure biocharleft: synchronous spectrum; middle: asynchronous spectrum; right: auto-correlation peak intensity graph
    Correlation spectra of biochars in 1 800~800 cm-1 band(a): Chicken manure biochar; (b): Cow dung biochar; (c): Pig manure biochar left: synchronous spectrum; middle: asynchronous spectrum; right: auto-correlation peak intensity graph
    Variation in relative intensities of groups
    • Table 1. Noda’s rules for peaks analysis

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      Table 1. Noda’s rules for peaks analysis

      Φ(v1,v2)Ψ(v1,v2)规则
      +nonev1, v2变化趋势一致(同增或同减)
      -nonev1, v2变化趋势不一致
      none+
      -
      无法判断
      ++v1变化先于v2
      +-v1变化晚于v2
      -+v1变化晚于v2
      --v1变化先于v2
    • Table 3. Group identification of biochar peak

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      Table 3. Group identification of biochar peak

      峰位置/cm-1基团归属参考文献
      3 415, 3 375, 3 350醇、 酚—OH
      3 045烯烃=C—H[20]
      2 930—CH2反对称伸缩[16]
      1 705, 1 655, 1 614, 1 605C=O[8]
      1 448, 1 440, 1 434C=C[16]
      1 380COO-[21]
      1 265, 1 235羧酸C—OH[17]
      1 108, 1 085, 1 045, 1 038多糖C—O或Si—O[17-18]
      976, 965, 957P—O/C—H[22]
      880C—H[16]
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    Xiang-yang GUI, Chen LIU, Ji-hong XU, Fang-lei DUAN, Shu-wei FANG, Fei-yue LI. Two-Dimensional Perturbation Correlation Infrared Spectroscopy Analysis of Animal Manure Biochar[J]. Spectroscopy and Spectral Analysis, 2020, 40(11): 3606

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    Paper Information

    Category: Research Articles

    Received: Sep. 9, 2019

    Accepted: --

    Published Online: Jun. 18, 2021

    The Author Email: GUI Xiang-yang (304134321@qq.com)

    DOI:10.3964/j.issn.1000-0593(2020)11-3606-07

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