Chinese Journal of Lasers, Volume. 51, Issue 10, 1002313(2024)

In-Situ Gradient Additive Forming and Interfacial Microstructure Evolution of Ti6Al4V/NiTi Heterogeneous Functional Material (Invited)

Jiali Gao1, Xu Wang1, Yunbo Hao2, Zhiqiang Wang1, and Kai Zhao2、*
Author Affiliations
  • 1College of Mechanical Engineering, University of Shanghai for Science and Technology, Shanghai 200093, China
  • 2Shanghai Aerospace Equipments Manufacturer Co., Ltd., Shanghai 200245, China
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    Figures & Tables(10)
    Transport diagram of heterogeneous alloy powder, as well as morphology and particle size distributions of two kinds of powders. (a) Schematic diagram of synchronous delivery of heterogeneous alloy powder; (b) micro-morphology of Ti6Al4V powder; (c) particle size distribution of Ti6Al4V powder; (d) micro-morphology of Ni55.5Ti44.5 powder; (e) particle size distribution of Ni55.5Ti44.5 powder
    Gradient compositional design of Ti6Al4V/NiTi heterogeneous alloy prepared by in-situ additive manufacturing
    XRD spectra and macroscopic morphology of Ti6Al4V/NiTi composites thin-walled samples with 11 compositional ratios. (a) XRD spectra; (b) macroscopic morphology
    Microstructures of Ti6Al4V/NiTi composites thin-walled samples with different composition ratios
    Elemental mass fraction changing of Ti6Al4V/NiTi thin-walled samples with different composition ratios
    In-situ gradient additive manufacturing of Ti6Al4V/NiTi heterogeneous functional materials. (a) Macroscopic morphology of formed part; (b) planer surface and partial enlargement of gradient transition zone of formed sample
    EDS line scan results near Ti6Al4V/NiTi gradient alloy interfaces. (a) Interfaces 1 and 2; (b) interface 3; (c) interface 4; (d) interface 5
    Schematic diagram of microhardness measurement points and distribution of measurement results for Ti6Al4V/NiTi gradient alloy. (a) Schematic diagram of sampling measurement points; (b) distribution of microhardness measurement results
    • Table 1. Process parameters corresponding to different composition ratios

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      Table 1. Process parameters corresponding to different composition ratios

      No.Ingredient ratio (mass fraction)P /WS /(mm/s)F /(g/min)

      FTi6Al4V /

      (g/min)

      FNiTi /

      (g/min)

      Interlayerlift /mmNumber ofprint layersSubstrate
      1100%Ti6Al4V12928.795.195.190.5618Ti6Al4V
      290%Ti6Al4V+10%NiTi12928.795.585.020.560.5318Ti6Al4V
      380%Ti6Al4V+20%NiTi12928.796.034.821.210.5418Ti6Al4V
      470%Ti6Al4V+30%NiTi12928.796.554.591.970.5618Ti6Al4V
      560%Ti6Al4V+40%NiTi12928.797.184.312.870.6116Ti6Al4V
      650%Ti6Al4V+50%NiTi12928.797.933.973.970.7514NiTi
      740%Ti6Al4V+60%NiTi12928.798.873.555.320.7812NiTi
      830%Ti6Al4V+70%NiTi12928.7910.053.027.040.7912NiTi
      920%Ti6Al4V+80%NiTi12928.7911.602.329.280.8512NiTi
      1010%Ti6Al4V+90%NiTi12928.7913.721.3712.350.9610NiTi
      11100%NiTi12928.7916.7816.781.268NiTi
    • Table 2. SEM observation and EDS analysis of Ti6Al4V/NiTi gradient alloy

      View table

      Table 2. SEM observation and EDS analysis of Ti6Al4V/NiTi gradient alloy

      SEM morphologyPositionAtomic fraction /%Possible phase
      TiNiAlV
      Region A46.352.41.00.3
      Point A147.451.80.50.3NiTi+Ni3Ti
      Point A246.752.80.30.2NiTi+Ni3Ti
      Region B48.350.80.70.2
      Point B148.151.00.50.4NiTi
      Region C49.549.40.80.3
      Point C155.542.01.31.2NiTi+NiTi2
      Region D53.544.71.00.8
      Point D153.743.91.50.9NiTi+NiTi2
      Region E54.543.11.31.1
      Point E153.943.91.30.8NiTi+NiTi2
      Region F262.134.81.81.3
      Point F261.535.32.01.2NiTi2
      Region F61.035.82.11.1
      Point F160.636.22.01.2NiTi2
      Region G61.235.62.21.1
      Point G161.735.71.61.0NiTi2
      Region H83.88.84.72.7
      Point H182.99.34.43.5α-Ti+NiTi2
      Region I90.70.15.24.0
      Point I191.005.33.7α-Ti+β-Ti
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    Jiali Gao, Xu Wang, Yunbo Hao, Zhiqiang Wang, Kai Zhao. In-Situ Gradient Additive Forming and Interfacial Microstructure Evolution of Ti6Al4V/NiTi Heterogeneous Functional Material (Invited)[J]. Chinese Journal of Lasers, 2024, 51(10): 1002313

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    Paper Information

    Category: Laser Additive Manufacturing

    Received: Jan. 2, 2024

    Accepted: Mar. 13, 2024

    Published Online: Apr. 27, 2024

    The Author Email: Zhao Kai (zkdlut@163.com)

    DOI:10.3788/CJL240435

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