Chinese Journal of Quantum Electronics, Volume. 41, Issue 5, 822(2024)

Synthesis and purification of novel infrared nonlinear BaGa4Se7 polycrystalline

ZHOU Qiang1...2,*, WANG Zhenyou1, WU Haixin1, HUANG Changbao1, NI Youbao1, YU Xuezhou1,2, HU Qianqian1,2, LIU Guojin1,2, and WEI Lingli12 |Show fewer author(s)
Author Affiliations
  • 1Anhui Provincial Key Laboratory of Photonic Devices and Materials, Anhui Institute of Optics and Fine Mechanics, HFIPS, Chinese Academy of Sciences, Hefei 230031, China
  • 2University of Science and Technology of China, Hefei 230026, China
  • show less
    Figures & Tables(8)
    Schematic diagram of two-temperature zone method
    Temperature curve of two-temperature zone method
    (a) BGSe polycrystalline Synthesized by two-temperature zone method; (b) BGSe polycrystalline Synthesized byhigh-pressure-assisted method
    XRD patterns of the BGSe samples. (a) Two-temperature zone method; (b) High-pressure-assisted method;(c) Purification; (d) Simulation
    Purified BGSe ingot
    SEM images of BGSe polycrystalline. (a) Before purification; (b) After purification
    EDS images of BGSe polycrystalline. (a) Before purification; (b) After purification
    • Table 2. ICP-MS test results for inorganic impurities in BGSe polycrystalline

      View table
      View in Article

      Table 2. ICP-MS test results for inorganic impurities in BGSe polycrystalline

      ImpurityA1/(mg⋅L-1)A2/%B1/(mg⋅L-1)B2/%C/%
      Fe0.16280.0045690520.07530.001956753.74%(↓)
      Al0.49130.0137847640.32440.008431334.97%(↓)
      Mn0.01470.0004129630.00250.000063082.99%(↓)
      Mg0.02040.0005720050.01750.000455514.21%(↓)
      Cr0.02240.0006279280.01570.000408629.91%(↓)
      Total0.71160.0199667120.43540.011315138.81%(↓)
    Tools

    Get Citation

    Copy Citation Text

    Qiang ZHOU, Zhenyou WANG, Haixin WU, Changbao HUANG, Youbao NI, Xuezhou YU, Qianqian HU, Guojin LIU, Lingli WEI. Synthesis and purification of novel infrared nonlinear BaGa4Se7 polycrystalline[J]. Chinese Journal of Quantum Electronics, 2024, 41(5): 822

    Download Citation

    EndNote(RIS)BibTexPlain Text
    Save article for my favorites
    Paper Information

    Category: Optical Material

    Received: Dec. 28, 2023

    Accepted: --

    Published Online: Jan. 8, 2025

    The Author Email:

    DOI:10.3969/j.issn.1007-5461.2024.05.012

    Topics