NUCLEAR TECHNIQUES, Volume. 48, Issue 2, 020101(2025)

Research and implementation of 2D X-ray diffraction data calibration

Bing GUO1,*... Shangming HE2, Jianbo MA2, Xiaoling WU1 and Fenggang BIAN2 |Show fewer author(s)
Author Affiliations
  • 1Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800, China
  • 2Shanghai Advanced Research Institute, Chinese Academy of Sciences, Shanghai 201204, China
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    Figures & Tables(8)
    Schematic diagram of sample diffraction experiment (a) Ideal experimental state, (b) Real experimental state
    Diffraction pattern of I-2θ before calibration
    Geometry used in pyFAI
    Illustration of calibration interface
    Comparison of calibration accuracy (a) Accurate calibration, (b) Inaccurate calibration
    Interface diagram of integral result
    Comparison of I-2θ data among uncalibrated, FIT2D, Dioptas and Corona after integrated (color online)
    • Table 1. The test results

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      Table 1. The test results

      软件 SoftwareSD / mmCenterX / pxCenterY / pxTilt / (°)Tilt Plan / (°)
      FIT2D158.5251 036.871995.0241.192159.943
      Dioptas158.5131 036.647995.1211.103159.699
      Corona158.5121 036.5651 052.807(995.193)1.094-160.218(160.218)
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    Bing GUO, Shangming HE, Jianbo MA, Xiaoling WU, Fenggang BIAN. Research and implementation of 2D X-ray diffraction data calibration[J]. NUCLEAR TECHNIQUES, 2025, 48(2): 020101

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    Paper Information

    Category: SYNCHROTRON RADIATION TECHNOLOGY AND APPLICATIONS

    Received: Dec. 19, 2023

    Accepted: --

    Published Online: Mar. 14, 2025

    The Author Email:

    DOI:10.11889/j.0253-3219.2025.hjs.48.230498

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