Acta Physica Sinica, Volume. 69, Issue 18, 187701-1(2020)

Preparation and ferroelectric domain structure of micro-scale piezoelectric array fabricated by Mn doped Pb(In1/2Nb1/2)O3-Pb(Mg1/3Nb2/3)O3-PbTiO3single crystal

Ju-Shan Wang1, Jin-Peng Ma1, Xiang-Yong Zhao1、*, Ming-Zhu Chen1, Fei-Fei Wang1, Tao Wang1, Yan-Xue Tang1, Wei Cheng1、*, Di Lin2, and Hao-Su Luo2
Author Affiliations
  • 1Mathematics and Science College, Shanghai Normal University, Shanghai 200234, China
  • 2Artificial Crystal Research Center, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 201899, China
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    Figures & Tables(10)
    Flow chart of the whole experiment.
    Results of lithography: (a), (b) Surface morphology under optical microscope and cross section under scanning electron microscope when the element size is 12.94 μm; (c), (d) surface morphology under optical microscope and cross section under scanning electron microscope when the element size is 13.97 μm.
    Schematic diagram of lithographic pattern structure.
    Electroplating experiment results: (a) Surface under scanning electron microscope; (b) cross section under scanning electron microscope.
    Etching rate experimental results: (a) Relationship between etching rate and antenna power; (b) relationship between etching rate and bias power; (c) relationship between etching rate and etching gas flow ratio.
    Etching results: (a) Surface morphology of high density array; (b) cross section morphology of high density array; (c) cross section morphology of conical array; (d) the surface morphology of deep etching of high density surface array.
    Structure of different scale areas under the piezoelectric microscope: (a) Surface morphology of 30 μm × 30 μm area; (b) out of plane amplitude of 30 μm × 30 μm area; (c) phase of 30 μm × 30 μm area; (d) surface morphology of 5 μm × 5 μm area; (e) out of plane amplitude of 5 μm × 5 μm area; (f) phase of 5 μm × 5 μm area; (g) surface morphology of 1 μm × 1 μm area; (h) out of plane amplitude of 1 μm × 1 μm area; (i) phase of 1 μm × 1 μm area.
    Results of 1 μm × 1 μm area under the piezoelectric force microscope: (a) Out of plane amplitude at ± 10 V; (b) phase at ± 10 V; (c) out of plane amplitude at ± 20 V; (d) phase at ± 20 V; (e) out of plane amplitude at ± 30 V; (f) phase at ± 30 V.
    Electric field induced amplitude and phase evolution in situ in the 1 μm × 1 μm area at room temperature
    • Table 1.

      Composition and content of electroplate bath ingredients.

      电镀液配料成分及含量

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      Table 1.

      Composition and content of electroplate bath ingredients.

      电镀液配料成分及含量

      成分含量
      氨基磺酸镍/g·L–1280—400
      硼酸/g·L–140—50
      阳极活化剂/g·L–160—100
      润湿剂/mL·L–11—5
      去应力剂适量
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    Ju-Shan Wang, Jin-Peng Ma, Xiang-Yong Zhao, Ming-Zhu Chen, Fei-Fei Wang, Tao Wang, Yan-Xue Tang, Wei Cheng, Di Lin, Hao-Su Luo. Preparation and ferroelectric domain structure of micro-scale piezoelectric array fabricated by Mn doped Pb(In1/2Nb1/2)O3-Pb(Mg1/3Nb2/3)O3-PbTiO3single crystal [J]. Acta Physica Sinica, 2020, 69(18): 187701-1

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    Paper Information

    Category:

    Received: Apr. 13, 2020

    Accepted: --

    Published Online: Jan. 5, 2021

    The Author Email: Cheng Wei (chengwei@shnu.edu.cn)

    DOI:10.7498/aps.69.20200544

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