Chinese Physics B, Volume. 29, Issue 9, (2020)

A double-layer heating method to generate high temperature in a two-stage multi-anvil apparatus

Bo Peng, Zili Kou, Mengxi Zhao, Mingli Jiang, Jiawei Zhang, Yipeng Wang, and Lu Zhang
Author Affiliations
  • Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, China
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    Figures & Tables(6)
    The R and R′ indicate the resistance of the heaters and the total resistance of the other part of the assemblies, respectively. P = I2(R + R′), under the same heating power, the total resistance decreases and the total current augments, which increases the heat generated in R′ and decreases the heat generated in the heaters. So the method of double-layer heaters can slow down the rapid rise of the cavity temperature.
    The schematic diagrams of two assemblies. (a) The schematic diagram of the DHA. Two layers of heaters were insulated by an aluminum tube, and the two heaters were connected with two 0.2 mm Ta electrodes in the assembly. (b) The schematic diagram of the SHA. It is a normal 10/4 assembly which is used widely.
    The power–temperature diagrams of assemblies. (a)–(c) The relationships for the sample diameters of 2.5 mm, 2.3 mm, and 2 mm, respectively. (d) The relationships for type No. 3 and type No. 11.
    The SEM images of recovered sample. (a) The image of recovered sample of the DHA (type No. 3). (b) Enlarged image of red circle in (a), the dendritic texture indicates the melting of the sample.
    • Table 1. Summary of the heating experiments. The sample size is given in the order of diameter and height. The size of the thermal insulator tube is given in the order of thickness and height.

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      Table 1. Summary of the heating experiments. The sample size is given in the order of diameter and height. The size of the thermal insulator tube is given in the order of thickness and height.

      AssemblyType No.Sample size/mmThickness of heater/mmSize of thermal insulator/mmP/GPaHighest temperature/°C
      DHA12.5/40.0250.85/4202000
      DHA22.3/40.0250.95/4202200
      DHA32/40.0251.1/4202500
      DHA42/30.0251.1/3202500
      SHA72.5/40.0250.85/4201800
      SHA82.3/40.0250.95/4201850
      SHA92/40.0251.1/4201950
      SHA102/30.0251.1/3202000
      SHA112/40.051.1/4201950
    • Table 2. The statistics of the temperatures and the average holding time of two assemblies.

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      Table 2. The statistics of the temperatures and the average holding time of two assemblies.

      AssemblyTemperature/°CHolding time
      Experiment timesLess than 3 min3–5 minOver 5 minAverage duration/min
      SHA2000104603.6
      DHA2000100645.3
      2300103703.2
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    Bo Peng, Zili Kou, Mengxi Zhao, Mingli Jiang, Jiawei Zhang, Yipeng Wang, Lu Zhang. A double-layer heating method to generate high temperature in a two-stage multi-anvil apparatus[J]. Chinese Physics B, 2020, 29(9):

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    Paper Information

    Received: Apr. 21, 2020

    Accepted: --

    Published Online: Apr. 29, 2021

    The Author Email: Kou Zili (kouzili@scu.edu.cn)

    DOI:10.1088/1674-1056/ab9dec

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